N¹-cinnamoylspermidine dihydrochloride

Base Information

Chemical Name:N¹-cinnamoylspermidine dihydrochloride
CAS No.:114643-54-8
Molecular Formula:C₂₄H₃₈N₄O₇*2ClH
Molecular Weight:567.51
Hs Code.:

N<sup>1</sup>-<p-(2-acetamido-2-deoxy-α-D-galactopyranosyl)oxy>cinnamoylspermidine dihydrochloride

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N¹-cinnamoylspermidine dihydrochloride

Chemical Property:

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Technology Process of N¹-cinnamoylspermidine dihydrochloride

There total 13 articles about N¹-cinnamoylspermidine dihydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67817-30-5
1,3,4,6-tetra-O-acetyl-2-azido-2-deoxy-alpha-D-galactopyranose

: 114643-54-8,114643-55-9
N¹-cinnamoylspermidine dihydrochloride

Guidance literature:: Multi-step reaction with 8 steps

1: HBr / CH₂Cl₂; acetic anhydride; acetic acid / 1 h / 0 °C

2: Et₄NCl

3: 55 percent / dimethylformamide / 65 h / Ambient temperature

4: quinoline, H₂ / 5percent Pd-BaSO₄ / methanol

5: pyridine

6: 78 percent / 90percent CF₃CO₂H / 1 h / Ambient temperature

7: 65 percent / carbonyldiimidazole / tetrahydrofuran / 20 h / Ambient temperature

8: NaOMe, HCl / methanol; diethyl ether

With pyridine; quinoline; hydrogenchloride; tetraethylammonium chloride; hydrogen bromide; hydrogen; sodium methylate; 1,1'-carbonyldiimidazole; trifluoroacetic acid; palladium on barium sulfate; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; acetic anhydride; acetic acid; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(87)80249-5

Reference yield:

: 67673-39-6
3,4,6-tri-O-acetyl-2-azido-2-deoxy-alpha-D-galactopyranosyl bromide

: 114643-54-8,114643-55-9
N¹-cinnamoylspermidine dihydrochloride

Guidance literature:: Multi-step reaction with 7 steps

1: Et₄NCl

2: 55 percent / dimethylformamide / 65 h / Ambient temperature

3: quinoline, H₂ / 5percent Pd-BaSO₄ / methanol

4: pyridine

5: 78 percent / 90percent CF₃CO₂H / 1 h / Ambient temperature

6: 65 percent / carbonyldiimidazole / tetrahydrofuran / 20 h / Ambient temperature

7: NaOMe, HCl / methanol; diethyl ether

With pyridine; quinoline; hydrogenchloride; tetraethylammonium chloride; hydrogen; sodium methylate; 1,1'-carbonyldiimidazole; trifluoroacetic acid; palladium on barium sulfate; In tetrahydrofuran; methanol; diethyl ether; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(87)80249-5

Reference yield:

: 114643-29-7
tert-butyl p-(3,4,6-tri-O-acetyl-2-azido-2-deoxy-α-D-galactopyranosyloxy)cinnamate

: 114643-54-8,114643-55-9
N¹-cinnamoylspermidine dihydrochloride

Guidance literature:: Multi-step reaction with 5 steps

1: quinoline, H₂ / 5percent Pd-BaSO₄ / methanol

2: pyridine

3: 78 percent / 90percent CF₃CO₂H / 1 h / Ambient temperature

4: 65 percent / carbonyldiimidazole / tetrahydrofuran / 20 h / Ambient temperature

5: NaOMe, HCl / methanol; diethyl ether

With pyridine; quinoline; hydrogenchloride; hydrogen; sodium methylate; 1,1'-carbonyldiimidazole; trifluoroacetic acid; palladium on barium sulfate; In tetrahydrofuran; methanol; diethyl ether;
DOI:10.1016/0008-6215(87)80249-5