C₇H₆BrClO₃S

Base Information

• Chemical Name: C₇H₆BrClO₃S
• CAS No.: 1261794-09-5
• Molecular Formula: C₇H₆BrClO₃S
• Molecular Weight: 285.546
• Mol file: 1261794-09-5.mol

Synonyms:

Chemical Property of C₇H₆BrClO₃S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₇H₆BrClO₃S

There total 1 articles about C₇H₆BrClO₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-bromo-2-methoxyphenylamine (116557-46-1) → C7H6BrClO3S (1261794-09-5)

Guidance literature:

3-bromo-2-methoxyphenylamine; With hydrogenchloride; sodium nitrite; In water; at 5 ℃;

With sulfur dioxide; acetic acid; copper(l) chloride; In water; at 20 ℃; for 2h;

DOI:10.1021/ml2000627

Reference yield:

C7H6BrClO3S (1261794-09-5) → C7H8BrNO3S (1261448-77-4)

Guidance literature:

With ammonia; In dichloromethane; at -78 - 20 ℃; for 2.16667h;

DOI:10.1021/ml2000627

Reference yield:

C7H6BrClO3S (1261794-09-5) → C17H28N2O4S

Guidance literature:

Multi-step reaction with 2 steps

1: ammonia / dichloromethane / 2.17 h / -78 - 20 °C

2: copper(l) iodide; potassium phosphate; L-proline / dimethyl sulfoxide / 120 °C / Microwave irradiation

With potassium phosphate; copper(l) iodide; ammonia; L-proline; In dichloromethane; dimethyl sulfoxide;

DOI:10.1021/ml2000627

upstream raw materials:

3-bromo-2-methoxyphenylamine

Downstream raw materials:

C₇H₈BrNO₃S