(+/–)-12(13)-DiHOME

Base Information

Chemical Name:(+/–)-12(13)-DiHOME
CAS No.:7293-40-5
Molecular Formula:C₁₈H₃₄O₄
Molecular Weight:314.466
Hs Code.:

Synonyms:

Suppliers and Price of (+/–)-12(13)-DiHOME

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/–)-12(13)-DiHOME

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (+/–)-12(13)-DiHOME

There total 1 articles about (+/–)-12(13)-DiHOME which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75452-47-0
methyl 9-iodononanoate

: 7293-40-5,23201-88-9,53734-71-7,59981-82-7,59981-83-8,59981-84-9,59981-85-0,73889-55-1
(12S,13R,Z)-12,13-dihydroxyoctadec-9-enoic acid

Guidance literature:: Multi-step reaction with 4 steps

1.1: acetonitrile / Reflux

2.1: sodium hexamethyldisilazane / tetrahydrofuran / 1 h / 0 °C

2.2: 6 h / -78 - 20 °C

3.1: toluene-4-sulfonic acid / methanol / 20 h / 40 °C

4.1: lithium hydroxide / methanol; tetrahydrofuran / 1 h / 20 °C

With sodium hexamethyldisilazane; toluene-4-sulfonic acid; lithium hydroxide; In tetrahydrofuran; methanol; acetonitrile; 2.1: |Wittig Olefination / 2.2: |Wittig Olefination;
DOI:10.1039/c7ob02291c

Reference yield:

: 7293-40-5,23201-88-9,53734-71-7,59981-82-7,59981-83-8,59981-84-9,59981-85-0,73889-55-1
(+/–)-12(13)-DiHOME

: 544-35-4
ethyl (9Z,12Z)-9,12-octadecadienoate

Guidance literature:: Multi-step reaction with 3 steps

1: (i) Br₂, (ii) HBr, AcOH, H₂SO₄

2: H₂SO₄

3: Zn, aq. HBr

With sulfuric acid; hydrogen bromide; zinc;
DOI:10.1039/jr9610004409