N,N'-1,2-acenaphthylenediylidene bis(2,6-dimethyl aniline) palladium(II)(κ2-CH(OAc)nPr) hexafluoroantimonate

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Chemical Name:N,N'-1,2-acenaphthylenediylidene bis(2,6-dimethyl aniline) palladium(II)(κ2-CH(OAc)nPr) hexafluoroantimonate
CAS No.:851539-90-7
Molecular Formula:C₃₄H₃₅N₂O₂Pd*F₆Sb
Molecular Weight:845.825
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N'-1,2-acenaphthylenediylidene bis(2,6-dimethyl aniline) palladium(II)(κ2-CH(OAc)nPr) hexafluoroantimonate

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Technology Process of N,N'-1,2-acenaphthylenediylidene bis(2,6-dimethyl aniline) palladium(II)(κ2-CH(OAc)nPr) hexafluoroantimonate

There total 1 articles about N,N'-1,2-acenaphthylenediylidene bis(2,6-dimethyl aniline) palladium(II)(κ2-CH(OAc)nPr) hexafluoroantimonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 26042-64-8
silver hexafluoroantimonate

: 591-87-7
Allyl acetate

: 185406-04-6
N,N'-1,2-acenaphthylenediylidene bis(2,6-dimethyl aniline) palladium(II) methyl chloride

: 851539-93-0
N,N'-1,2-acenaphthylenediylidene bis(2,6-dimethyl aniline) palladium(II)(κ2-CH(OAc)iPr) hexafluoroantimonate

: 851539-90-7
N,N'-1,2-acenaphthylenediylidene bis(2,6-dimethyl aniline) palladium(II)(κ2-CH(OAc)nPr) hexafluoroantimonate

Guidance literature:: In diethyl ether; dichloromethane; byproducts: AgCl; (Ar), Pd complex and AgSbF6 cooled to -78°C, treated with dry CH2Cl2, ether and allyl acetate, warmed to -25°C for 1.5 h, warmed to room temp. for 1 h; filtered, evapd.(vac.), crystd.(THF/ether) at -30°C, elem. anal.; Kinetics;
DOI:10.1021/ja045969s