mer-trans-[2-(diphenylphosphanyl)-3-ethylphenyl-C⁽¹⁾,P](iodo)(methyl)bis(trimethylphosphane)cobalt

Base Information

• Chemical Name: mer-trans-[2-(diphenylphosphanyl)-3-ethylphenyl-C⁽¹⁾,P](iodo)(methyl)bis(trimethylphosphane)cobalt
• CAS No.: 561328-19-6
• Molecular Formula: C₂₇H₃₉CoIP₃
• Molecular Weight: 642.426

Synonyms:

Chemical Property of mer-trans-[2-(diphenylphosphanyl)-3-ethylphenyl-C⁽¹⁾,P](iodo)(methyl)bis(trimethylphosphane)cobalt

Chemical Property:

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Technology Process of mer-trans-[2-(diphenylphosphanyl)-3-ethylphenyl-C⁽¹⁾,P](iodo)(methyl)bis(trimethylphosphane)cobalt

There total 1 articles about mer-trans-[2-(diphenylphosphanyl)-3-ethylphenyl-C⁽¹⁾,P](iodo)(methyl)bis(trimethylphosphane)cobalt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

[2-(diphenylphosphanyl)-3-ethylphenyl-C(1),P]tris(trimethylphosphane)cobalt (561328-07-2) + methyl iodide (74-88-4) → mer-trans-[2-(diphenylphosphanyl)-3-ethylphenyl-C(1),P](iodo)(methyl)bis(trimethylphosphane)cobalt (561328-19-6)

Guidance literature:

In diethyl ether; byproducts: tetramethylphosphonium iodide; soln. of Co complex in Et2O combined at -70°C with MeI, allowed to warm to 20°C; filtered after 3 h, crystd. from filtrate at -27°C; elem. anal.;

DOI:10.1002/ejic.200390115

upstream raw materials:

[2-(diphenylphosphanyl)-3-ethylphenyl-C⁽¹⁾,P]tris(trimethylphosphane)cobalt

methyl iodide

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