C₃₈H₅₇NO₁₀SSi

Base Information

Chemical Name:C₃₈H₅₇NO₁₀SSi
CAS No.:685885-62-5
Molecular Formula:C₃₈H₅₇NO₁₀SSi
Molecular Weight:748.023
Hs Code.:

C<sub>38</sub>H<sub>57</sub>NO<sub>10</sub>SSi

Synonyms:

Suppliers and Price of C₃₈H₅₇NO₁₀SSi

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₃₈H₅₇NO₁₀SSi

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₃₈H₅₇NO₁₀SSi

There total 17 articles about C₃₈H₅₇NO₁₀SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 524734-72-3
[(4R,5S)-2,2,5-Trimethyl-5-((R)-3-oxo-1-triethylsilanyloxy-propyl)-[1,3]dioxolan-4-yl]-acetonitrile

: 685885-62-5
C₃₈H₅₇NO₁₀SSi

Guidance literature:: Multi-step reaction with 11 steps

1: n-BuLi / tetrahydrofuran

2: TBAF / tetrahydrofuran

3: 99 percent / CuI; n-PrNH₂ / Pd(PPh₃)4 / toluene

4: 100 percent / pyridine; DMAP / CH₂Cl₂

5: HF*pyridine / acetonitrile

6: BF₃*OEt₂ / CH₂Cl₂

7: 93 percent / pyridine / dimethylformamide / 48 h / 0 - 20 °C

8: 83 percent / n-BuLi / tetrahydrofuran / 1.25 h / -78 °C

9: CSA / methanol / 6 h / 20 °C

10: toluene / 85 °C

With pyridine; propylamine; dmap; copper(l) iodide; n-butyllithium; camphor-10-sulfonic acid; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; pyridine hydrogenfluoride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1055/s-2004-817769

Reference yield:

: 1-((2S,3R,5S,6R)-3-Hydroxy-5-methoxy-6-methoxymethyl-tetrahydro-pyran-2-yl)-propan-2-one

: 685885-62-5
C₃₈H₅₇NO₁₀SSi

Guidance literature:: Multi-step reaction with 11 steps

1.1: PPTS / CH₂Cl₂

2.1: LDA / tetrahydrofuran / -78 °C

2.2: tetrahydrofuran / 20 °C

2.3: CSA / methanol

3.1: 99 percent / CuI; n-PrNH₂ / Pd(PPh₃)4 / toluene

4.1: 100 percent / pyridine; DMAP / CH₂Cl₂

5.1: HF*pyridine / acetonitrile

6.1: BF₃*OEt₂ / CH₂Cl₂

7.1: 93 percent / pyridine / dimethylformamide / 48 h / 0 - 20 °C

8.1: 83 percent / n-BuLi / tetrahydrofuran / 1.25 h / -78 °C

9.1: CSA / methanol / 6 h / 20 °C

10.1: toluene / 85 °C

With pyridine; propylamine; dmap; copper(l) iodide; n-butyllithium; camphor-10-sulfonic acid; boron trifluoride diethyl etherate; pyridinium p-toluenesulfonate; pyridine hydrogenfluoride; lithium diisopropyl amide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1055/s-2004-817769

Reference yield:

: 685885-52-3
(3R,5S,6R)-3-Benzyloxy-5-methoxy-6-methoxymethyl-tetrahydro-pyran-2-one

: 685885-62-5
C₃₈H₅₇NO₁₀SSi

Guidance literature:: Multi-step reaction with 14 steps

1.1: tetrahydrofuran

1.2: 64 percent / Et₃SiH; BF₃*OEt₂ / acetonitrile

2.1: O₂; aq. CuCl / PdCl₂ / dimethylformamide

3.1: H₂ / Pd/C / ethanol

4.1: PPTS / CH₂Cl₂

5.1: LDA / tetrahydrofuran / -78 °C

5.2: tetrahydrofuran / 20 °C

5.3: CSA / methanol

6.1: 99 percent / CuI; n-PrNH₂ / Pd(PPh₃)4 / toluene

7.1: 100 percent / pyridine; DMAP / CH₂Cl₂

8.1: HF*pyridine / acetonitrile

9.1: BF₃*OEt₂ / CH₂Cl₂

10.1: 93 percent / pyridine / dimethylformamide / 48 h / 0 - 20 °C

11.1: 83 percent / n-BuLi / tetrahydrofuran / 1.25 h / -78 °C

12.1: CSA / methanol / 6 h / 20 °C

13.1: toluene / 85 °C

With pyridine; propylamine; dmap; copper(l) iodide; n-butyllithium; camphor-10-sulfonic acid; boron trifluoride diethyl etherate; hydrogen; oxygen; pyridinium p-toluenesulfonate; pyridine hydrogenfluoride; copper(l) chloride; lithium diisopropyl amide; palladium on activated charcoal; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium dichloride; In tetrahydrofuran; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide; toluene; acetonitrile; 1.2: Kishi's reduction / 2.1: Wacker oxidation;
DOI:10.1055/s-2004-817769