tert-butyl 7β-<2-(2-tritylaminothiazol-4-yl)-(Z)-2-methoxyiminoacetamido>-3-<(5-methyl-1,3,4-thiadiazol-2-yl)thio>-1-dethia-2-thia-3-cephem-4-carboxylate

Base Information

Chemical Name:tert-butyl 7β-<2-(2-tritylaminothiazol-4-yl)-(Z)-2-methoxyiminoacetamido>-3-<(5-methyl-1,3,4-thiadiazol-2-yl)thio>-1-dethia-2-thia-3-cephem-4-carboxylate
CAS No.:102142-90-5
Molecular Formula:C₃₉H₃₇N₇O₅S₄
Molecular Weight:812.031
Hs Code.:

tert-butyl 7β-<2-(2-tritylaminothiazol-4-yl)-(Z)-2-methoxyiminoacetamido>-3-<(5-methyl-1,3,4-thiadiazol-2-yl)thio>-1-dethia-2-thia-3-cephem-4-carboxylate

Synonyms:

Suppliers and Price of tert-butyl 7β-<2-(2-tritylaminothiazol-4-yl)-(Z)-2-methoxyiminoacetamido>-3-<(5-methyl-1,3,4-thiadiazol-2-yl)thio>-1-dethia-2-thia-3-cephem-4-carboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of tert-butyl 7β-<2-(2-tritylaminothiazol-4-yl)-(Z)-2-methoxyiminoacetamido>-3-<(5-methyl-1,3,4-thiadiazol-2-yl)thio>-1-dethia-2-thia-3-cephem-4-carboxylate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of tert-butyl 7β-<2-(2-tritylaminothiazol-4-yl)-(Z)-2-methoxyiminoacetamido>-3-<(5-methyl-1,3,4-thiadiazol-2-yl)thio>-1-dethia-2-thia-3-cephem-4-carboxylate

There total 3 articles about tert-butyl 7β-<2-(2-tritylaminothiazol-4-yl)-(Z)-2-methoxyiminoacetamido>-3-<(5-methyl-1,3,4-thiadiazol-2-yl)thio>-1-dethia-2-thia-3-cephem-4-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.7%

: 102142-89-2,124918-17-8,124918-18-9
tert-butyl 7β-<2-(2-tritylaminothiazol-4-yl)-(Z)-2-methoxyiminoacetamido>-3-<(5-methyl-1,3,4-thiadiazol-2-yl)thio>-4-hydroxy-1-dethia-2-thiacepham-4-carboxylate

: 102062-23-7
(6S,7S)-7-{2-[(Z)-Methoxyimino]-2-[2-(trityl-amino)-thiazol-4-yl]-acetylamino}-8-oxo-4-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid tert-butyl ester

: 102142-90-5,124918-25-8
tert-butyl 7β-<2-(2-tritylaminothiazol-4-yl)-(Z)-2-methoxyiminoacetamido>-3-<(5-methyl-1,3,4-thiadiazol-2-yl)thio>-1-dethia-2-thia-3-cephem-4-carboxylate

Guidance literature:: With diphosphorus tetraiodide; In pyridine;
DOI:10.3987/COM-88-S127

Reference yield:

: 71901-63-8
tert-butyl diazopyruvate

: 102142-90-5,124918-25-8
tert-butyl 7β-<2-(2-tritylaminothiazol-4-yl)-(Z)-2-methoxyiminoacetamido>-3-<(5-methyl-1,3,4-thiadiazol-2-yl)thio>-1-dethia-2-thia-3-cephem-4-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: CH₂Cl₂ / 1 h / Ambient temperature

2: Et₃N / CH₂Cl₂ / 2 h / Ambient temperature

3: 26.7 percent / P₂I₄ / pyridine

With diphosphorus tetraiodide; triethylamine; In pyridine; dichloromethane;
DOI:10.3987/COM-88-S127

Reference yield:

: 124831-43-2
tert-Butyl 2-oxo-3-chloro-3-<(5-methyl-1,3,4-thiadiazol-2-yl)thio>propanoate

: 102142-90-5,124918-25-8
tert-butyl 7β-<2-(2-tritylaminothiazol-4-yl)-(Z)-2-methoxyiminoacetamido>-3-<(5-methyl-1,3,4-thiadiazol-2-yl)thio>-1-dethia-2-thia-3-cephem-4-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / CH₂Cl₂ / 2 h / Ambient temperature

2: 26.7 percent / P₂I₄ / pyridine

With diphosphorus tetraiodide; triethylamine; In pyridine; dichloromethane;
DOI:10.3987/COM-88-S127