(3S,4S)-3-pentyl-6-tosyloxyhexan-4-olide

Base Information

Chemical Name:(3S,4S)-3-pentyl-6-tosyloxyhexan-4-olide
CAS No.:155016-10-7
Molecular Formula:C₁₈H₂₆O₅S
Molecular Weight:354.467
Hs Code.:

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Chemical Property of (3S,4S)-3-pentyl-6-tosyloxyhexan-4-olide

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Technology Process of (3S,4S)-3-pentyl-6-tosyloxyhexan-4-olide

There total 8 articles about (3S,4S)-3-pentyl-6-tosyloxyhexan-4-olide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.3%

: 98-59-9
p-toluenesulfonyl chloride

: 155016-09-4
(3S,4S)-6-hydroxy-3-pentyl-4-hexanolide

: 155016-10-7
(3S,4S)-3-pentyl-6-tosyloxyhexan-4-olide

Guidance literature:: With pyridine; Ambient temperature;

Reference yield:

: 37112-31-5
levoglucosenone

: 155016-10-7
(3S,4S)-3-pentyl-6-tosyloxyhexan-4-olide

Guidance literature:: Multi-step reaction with 6 steps

1: 81 percent / CuI / diethyl ether / 3.5 h / -30 °C

2: 86.6 percent / pyridine / 3.5 h / Ambient temperature

3: 76.1 percent / K₂CO₃ / 50 °C

4: 1.) CuI, 2.) 10percent aq. NaOH / 1.) ether, -20 deg C, 30 min, 2.) MeOH, RT, 3 h

5: 1.) O₃, 2.) borane-dimethyl sulfide complex, 3.) 5percent aq. HCl

6: 82.3 percent / pyridine / Ambient temperature

With pyridine; hydrogenchloride; sodium hydroxide; copper(l) iodide; dimethylsulfide borane complex; potassium carbonate; ozone; In diethyl ether;

Reference yield:

: 3525-31-3
n-pentyl lithium

: 155016-10-7
(3S,4S)-3-pentyl-6-tosyloxyhexan-4-olide

Guidance literature:: Multi-step reaction with 6 steps

1: 81 percent / CuI / diethyl ether / 3.5 h / -30 °C

2: 86.6 percent / pyridine / 3.5 h / Ambient temperature

3: 76.1 percent / K₂CO₃ / 50 °C

4: 1.) CuI, 2.) 10percent aq. NaOH / 1.) ether, -20 deg C, 30 min, 2.) MeOH, RT, 3 h

5: 1.) O₃, 2.) borane-dimethyl sulfide complex, 3.) 5percent aq. HCl

6: 82.3 percent / pyridine / Ambient temperature

With pyridine; hydrogenchloride; sodium hydroxide; copper(l) iodide; dimethylsulfide borane complex; potassium carbonate; ozone; In diethyl ether;