C₃₆H₄₃N₅O₈

Base Information

Chemical Name:C₃₆H₄₃N₅O₈
CAS No.:1610041-01-4
Molecular Formula:C₃₆H₄₃N₅O₈
Molecular Weight:673.766
Hs Code.:

C<sub>36</sub>H<sub>43</sub>N<sub>5</sub>O<sub>8</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₆H₄₃N₅O₈

Chemical Property:

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Technology Process of C₃₆H₄₃N₅O₈

There total 4 articles about C₃₆H₄₃N₅O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 862195-40-2
Z-Gly-Phe(2Me)-OH

: 1610040-83-9
C₁₆H₂₃N₃O₄

: 1610041-01-4
C₃₆H₄₃N₅O₈

: 1610041-00-3
C₃₆H₄₃N₅O₈

Guidance literature:: With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 15h; Overall yield = 91 %;
DOI:10.1002/hlca.201400084

Reference yield:

: Z-Gly-Aib-N(Me)Ph

: 1610041-01-4
C₃₆H₄₃N₅O₈

: 1610041-00-3
C₃₆H₄₃N₅O₈

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogenchloride / tetrahydrofuran; water / 20 °C

2: N-ethyl-N,N-diisopropylamine; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate / dichloromethane / 15 h / 20 °C

3: palladium 10% on activated carbon; hydrogen / methanol / 20 °C

4: N-ethyl-N,N-diisopropylamine; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate / dichloromethane / 15 h / 20 °C

With hydrogenchloride; palladium 10% on activated carbon; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; hydrogen; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1002/hlca.201400084

Reference yield:

: 2420-11-3
Z-Gly-Aib-OH

: 1610041-01-4
C₃₆H₄₃N₅O₈

: 1610041-00-3
C₃₆H₄₃N₅O₈

Guidance literature:: Multi-step reaction with 3 steps

1: N-ethyl-N,N-diisopropylamine; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate / dichloromethane / 15 h / 20 °C

2: palladium 10% on activated carbon; hydrogen / methanol / 20 °C

3: N-ethyl-N,N-diisopropylamine; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate / dichloromethane / 15 h / 20 °C

With palladium 10% on activated carbon; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; hydrogen; N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane;
DOI:10.1002/hlca.201400084