trans-diiodo(1,8-dimethyl-2-phenyl-imidazol-3-ylidene[1,2-a]pyridine)(pyridine)palladium(II)

Base Information

Chemical Name:trans-diiodo(1,8-dimethyl-2-phenyl-imidazol-3-ylidene[1,2-a]pyridine)(pyridine)palladium(II)
CAS No.:1204776-69-1
Molecular Formula:C₂₀H₁₉I₂N₃Pd
Molecular Weight:661.62
Hs Code.:

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Chemical Property of trans-diiodo(1,8-dimethyl-2-phenyl-imidazol-3-ylidene[1,2-a]pyridine)(pyridine)palladium(II)

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Technology Process of trans-diiodo(1,8-dimethyl-2-phenyl-imidazol-3-ylidene[1,2-a]pyridine)(pyridine)palladium(II)

There total 1 articles about trans-diiodo(1,8-dimethyl-2-phenyl-imidazol-3-ylidene[1,2-a]pyridine)(pyridine)palladium(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 110-86-1
pyridine

: 1204776-65-7,4598-06-5
1,8-dimethyl-2-phenyl-imidazo[1,2-a]pyridin-1-ium iodide

: palladium dichloride

: 1204776-69-1
trans-diiodo(1,8-dimethyl-2-phenyl-imidazol-3-ylidene[1,2-a]pyridine)(pyridine)palladium(II)

Guidance literature:: With K₂CO₃; In pyridine; using standard Schlenk techniques; mixt. of ligand salt, PdCl2 and K2CO3in pyridine stirred at reflux for 16 h; cooled to room temp.; diluted with CHCl3; washed with aq. CuSO4 soln.; org. layer sepd.; dried(anhyd. MgSO4); concd. under vac.; solid isolated; elem. anal.;
DOI:10.1039/b913068c