C₂₃H₂₉N₃O₃

Base Information

Chemical Name:C₂₃H₂₉N₃O₃
CAS No.:1316848-30-2
Molecular Formula:C₂₃H₂₉N₃O₃
Molecular Weight:395.502
Hs Code.:

C<sub>23</sub>H<sub>29</sub>N<sub>3</sub>O<sub>3</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₃H₂₉N₃O₃

Chemical Property:

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Technology Process of C₂₃H₂₉N₃O₃

There total 9 articles about C₂₃H₂₉N₃O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1316848-29-9
(5S)-1-((3S)-1-(2-benzyl-5-oxo-2,5-dihydro-1H-pyrrol-3-yl)pyrrolidin-3-yl)-4-(tert-butoxy)-5-isobutyl-1H-pyrrol-2(5H)-one

: 1316848-30-2
C₂₃H₂₉N₃O₃

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 25 ℃; for 3h; Inert atmosphere;
DOI:10.1021/ja2033734

Reference yield:

: 1316848-06-2
C₂₂H₃₄N₂O₄*ClH

: 1316848-30-2
C₂₃H₂₉N₃O₃

Guidance literature:: Multi-step reaction with 4 steps

1: tetrahydrofuran / 3 h / 75 °C / Inert atmosphere

2: palladium 10% on activated carbon; hydrogen / methanol / 12 h / 25 °C / 760.05 Torr / Inert atmosphere

3: trimethyl orthoformate / isopropyl alcohol / 5 h / 25 °C / Inert atmosphere

4: trifluoroacetic acid / dichloromethane / 3 h / 25 °C / Inert atmosphere

With palladium 10% on activated carbon; hydrogen; trifluoroacetic acid; trimethyl orthoformate; In tetrahydrofuran; methanol; dichloromethane; isopropyl alcohol;
DOI:10.1021/ja2033734

Reference yield:

: 13734-34-4
N-tert-butoxycarbonyl-L-phenylalanine

: 1316848-30-2
C₂₃H₂₉N₃O₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 14 h / 0 - 25 °C / Inert atmosphere

1.2: 0.5 h / Inert atmosphere; Reflux

2.1: trifluoroacetic acid / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

3.1: trimethyl orthoformate / isopropyl alcohol / 5 h / 25 °C / Inert atmosphere

4.1: trifluoroacetic acid / dichloromethane / 3 h / 25 °C / Inert atmosphere

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; trimethyl orthoformate; In dichloromethane; isopropyl alcohol;
DOI:10.1021/ja2033734