Me₃Sn(4,5-dimethoxy-2-nitrobenzoate)

Base Information

• Chemical Name: Me₃Sn(4,5-dimethoxy-2-nitrobenzoate)
• CAS No.: 1229818-06-7
• Molecular Formula: C₁₂H₁₇NO₆Sn
• Molecular Weight: 389.98
• Mol file: 1229818-06-7.mol

Synonyms:

Chemical Property of Me₃Sn(4,5-dimethoxy-2-nitrobenzoate)

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of Me₃Sn(4,5-dimethoxy-2-nitrobenzoate)

There total 1 articles about Me₃Sn(4,5-dimethoxy-2-nitrobenzoate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

4,5-dimethoxy-2-nitro-benzoic acid (4998-07-6) + trimethyltin(IV)chloride (1066-45-1) → Me3Sn(4,5-dimethoxy-2-nitrobenzoate) (1229818-06-7)

Guidance literature:

With Et₃N; In chloroform; byproducts: Et3NHCl; Et3N (1 mmol) was added to dissolved in CHCl3 HL (1 mmol), mixt. was refluxed 30 min, 1 mmol Me3SnCl was added, solution was refluxed for 4-7 h,mixt. was kept at 20°C overnight; Et3NHCl was filtered off, solvent was evapd. under redused pressure, mass was crystd. from CHCl3:n-hexane (1:1); elem. anal.;

DOI:10.1134/S1070328409120069

upstream raw materials:

4,5-dimethoxy-2-nitro-benzoic acid

trimethyltin(IV)chloride