Technology Process of 1-(4-(benzylseleninyl)phenyl)ethanone
There total 3 articles about 1-(4-(benzylseleninyl)phenyl)ethanone which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
D-glucose 6-phosphate; Leuconostoc mesenteroides glucose-6-phosphate dehydrogenase; Thermobifida fuska recombinant phenylacetone monooxygenase; oxygen; NADPH;
In
dimethyl sulfoxide;
at 30 ℃;
for 24h;
pH=9;
chemoselective reaction;
aq. buffer;
Enzymatic reaction;
DOI:10.1016/j.molcatb.2011.07.018
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium tetrahydroborate / methanol / 0 °C
2: Leuconostoc mesenteroides glucose-6-phosphate dehydrogenase; Thermobifida fuska recombinant phenylacetone monooxygenase; D-glucose 6-phosphate; oxygen; NADPH / dimethyl sulfoxide / 24 h / 30 °C / pH 9 / aq. buffer; Enzymatic reaction
With
sodium tetrahydroborate; D-glucose 6-phosphate; Leuconostoc mesenteroides glucose-6-phosphate dehydrogenase; Thermobifida fuska recombinant phenylacetone monooxygenase; oxygen; NADPH;
In
methanol; dimethyl sulfoxide;
DOI:10.1016/j.molcatb.2011.07.018
- Guidance literature:
-
Multi-step reaction with 3 steps
1: hydrogenchloride; sodium nitrite / water
2: sodium tetrahydroborate / methanol / 0 °C
3: Leuconostoc mesenteroides glucose-6-phosphate dehydrogenase; Thermobifida fuska recombinant phenylacetone monooxygenase; D-glucose 6-phosphate; oxygen; NADPH / dimethyl sulfoxide / 24 h / 30 °C / pH 9 / aq. buffer; Enzymatic reaction
With
hydrogenchloride; sodium tetrahydroborate; D-glucose 6-phosphate; Leuconostoc mesenteroides glucose-6-phosphate dehydrogenase; Thermobifida fuska recombinant phenylacetone monooxygenase; oxygen; NADPH; sodium nitrite;
In
methanol; water; dimethyl sulfoxide;
DOI:10.1016/j.molcatb.2011.07.018
