cis-[Pt(NO₃)2(PMe₂Ph)2]

Base Information

• Chemical Name: cis-[Pt(NO₃)2(PMe₂Ph)2]
• CAS No.: 58320-37-9
• Molecular Formula: C₁₆H₂₂N₂O₆P₂Pt
• Molecular Weight: 595.388

Synonyms:

Chemical Property of cis-[Pt(NO₃)2(PMe₂Ph)2]

Chemical Property:

Purity/Quality:

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Technology Process of cis-[Pt(NO₃)2(PMe₂Ph)2]

There total 1 articles about cis-[Pt(NO₃)2(PMe₂Ph)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cis-[bis(dimethylphenylphosphane)dichlroplatinum(II)] (15393-14-3) → cis-[Pt(NO3)2(PMe2Ph)2] (58320-37-9)

Guidance literature:

With AgNO₃; In methanol; dichloromethane; byproducts: AgCl; addn. of 2 equiv. AgNO3 (in hot MeOH) to Pt-complex (in CH2Cl2), stirring for 2 h; filtration off of AgCl, evapn., recrystn. (MeOH); elem. anal.;

DOI:10.1039/DT9770001219

Reference yield:

PtMe(4-MeC6H4)(1,5-cyclooctadiene) (66485-00-5) + cis-[Pt(NO3)2(PMe2Ph)2] (58320-37-9) → trans-[Pt(NO3)(4-MeC6H4)(PMe2Ph)2] (79735-34-5)

Guidance literature:

In chloroform-d1; byproducts: [Pt(NO3)Me(1,5-cyclooctadiene)]; the soln. was sealed in an NMR tube, kept in the dark at 25°C for 4 d;

DOI:10.1021/ic00131a061

Reference yield:

cis-[Pt(NO3)2(PMe2Ph)2] (58320-37-9) + 4-tolyltrimethylstannane (937-12-2) → trans-[Pt(NO3)(4-MeC6H4)(PMe2Ph)2] (79735-34-5)

Guidance literature:

In dichloromethane; reflux for 1 d; the volume of soln. was reduced to yield crystals, washed with ether, elem. anal.;

DOI:10.1021/ic00131a061

upstream raw materials:

cis-[bis(dimethylphenylphosphane)dichlroplatinum(II)]

Downstream raw materials:

trans-[Pt(NO₃)(4-MeC₆H₄)(PMe₂Ph)2]

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