1,2-bisethane

Base Information

Chemical Name:1,2-bisethane
CAS No.:98815-26-0
Molecular Formula:C₂₆H₂₀Cl₄P₂
Molecular Weight:536.204
Hs Code.:

1,2-bis<bis(p-chlorophenyl)phosphino>ethane

Synonyms:

Suppliers and Price of 1,2-bisethane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,2-bisethane

Chemical Property:

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Technology Process of 1,2-bisethane

There total 1 articles about 1,2-bisethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 106-39-8
bromochlorobenzene

: 28240-69-9
1,2-bis(dichlorophosphino)ethane

: 98815-26-0
1,2-bisethane

Guidance literature:: With n-butyllithium; Yield given. Multistep reaction; 1) hexane, Et₂O, RT, 2 h; 2) hexane, Et₂O, 20 deg C, 1 h;
DOI:10.1039/DT9850001131

Reference yield: 85.0%

: 36151-25-4,36216-20-3
[WCl₄(P(C₆H₅)3)2]

: 98815-26-0
1,2-bisethane

: [WCl₄((ClC₆H₄)2PCH₂CH₂P(C₆H₄Cl)2)]

Guidance literature:: In benzene; (N2 or Ar); complex added to ligand soln., refluxed for 1 h; filtered off, dried in vac.;
DOI:10.1039/DT9840001703

Reference yield: 45.0%

: rhenum(V) dichloro-η2-benzoylhydrazido(3-) bis(triphenylphosphine)

: 98815-26-0
1,2-bisethane

: 98814-93-8
bis{1,2-bis(di-p-chlorophenylphosphino)ethane}chloro(dinitrogen)rhenium(I)

Guidance literature:: In methanol; suspension of (N-benzoylhydrazido(3-)-N',O)dichlorobis(triphenylphosphine)rhenium(V) and diphosphine in MeOH was heated to reflux for 4 h under N2;; filtration, filtrate taken to dryness, ether was added, yellow solid in benzene was heated under reflux for 1 h, soln. was reduced, ether was added; elem. anal.;;
DOI:10.1039/DT9850001131