FeCl₃*1,5-diphenyl 2,4-dithiobiuret

Base Information

• Chemical Name: FeCl₃*1,5-diphenyl 2,4-dithiobiuret
• CAS No.: 89485-27-8
• Molecular Formula: C₁₄H₁₃N₃S₂*Cl₃Fe
• Molecular Weight: 449.615
• Mol file: 89485-27-8.mol

Synonyms:

Chemical Property of FeCl₃*1,5-diphenyl 2,4-dithiobiuret

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of FeCl₃*1,5-diphenyl 2,4-dithiobiuret

There total 1 articles about FeCl₃*1,5-diphenyl 2,4-dithiobiuret which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,5-diphenyl-2,4-dithiobiuret (33951-45-0) + iron(III) chloride (7705-08-0) → FeCl3*1,5-diphenyl 2,4-dithiobiuret (89485-27-8)

Guidance literature:

With ammonium molybdate; NaOH; In nitrobenzene; ligand, ammonium molybdate were taken in flask, FeCl3 was transferred to flask, nitrobenzene was added, heated at 150°C for half and hour, then flask was heated at 200°C for 4 h, mixt. was cooled, filtered, washed with H2O; crude ppt. was treated with NaOH in H2O, distilled, neutralized with HCl and heated at 70°C for 1 h, filtered off, washed with H2O, extd. with acetone, heated at 170°C (1E-3 mm Hg); elem. anal.;

DOI:10.1016/S0277-5387(00)84709-9

upstream raw materials:

1,5-diphenyl-2,4-dithiobiuret

iron(III) chloride