C₂₄H₂₂Cl₂FN₃O

Base Information

Chemical Name:C₂₄H₂₂Cl₂FN₃O
CAS No.:955407-82-6
Molecular Formula:C₂₄H₂₂Cl₂FN₃O
Molecular Weight:458.363
Hs Code.:

C<sub>24</sub>H<sub>22</sub>Cl<sub>2</sub>FN<sub>3</sub>O

Synonyms:

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Chemical Property of C₂₄H₂₂Cl₂FN₃O

Chemical Property:

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Technology Process of C₂₄H₂₂Cl₂FN₃O

There total 9 articles about C₂₄H₂₂Cl₂FN₃O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 955373-73-6
(R)-4-((R)-4-benzyl-2-oxo-oxazolidin-3-yl)-3-(4-benzyloxy-2,6-dichloro-benzyl)-4-oxo-butyraldehyde

: 955407-81-5
C₂₄H₂₂Cl₂FN₃O

: 955407-82-6
C₂₄H₂₂Cl₂FN₃O

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 13 h / 20 - 50 °C

2.1: hydrogen / 10 % Pd(OH)2/C / ethanol / 3 h / 20 °C / 2585.81 Torr

3.1: pyridine / dichloromethane / 0.83 h / 0 - 20 °C

4.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran; water / 1 h / 60 - 80 °C

4.2: 20 °C

5.1: lithium hydroxide; water / tetrahydrofuran / 1 h / 20 °C

6.1: n-heptane; isopropyl alcohol / Resolution of racemate

With pyridine; lithium hydroxide; water; hydrogen; sodium tris(acetoxy)borohydride; sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 10 % Pd(OH)2/C; In tetrahydrofuran; ethanol; n-heptane; dichloromethane; water; 1,2-dichloro-ethane; isopropyl alcohol;

Reference yield:

: 955373-72-5
(R)-4-benzyl-3-[(S)-2-(4-benzyloxy-2,6-dichloro-benzyl)-pent-4-enoyl]-oxazolidin-2-onecf

: 955407-81-5
C₂₄H₂₂Cl₂FN₃O

: 955407-82-6
C₂₄H₂₂Cl₂FN₃O

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium periodate / osmium(VIII) oxide / tetrahydrofuran; water; tert-butyl alcohol / 4 h / 20 °C

2.1: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 13 h / 20 - 50 °C

3.1: hydrogen / 10 % Pd(OH)2/C / ethanol / 3 h / 20 °C / 2585.81 Torr

4.1: pyridine / dichloromethane / 0.83 h / 0 - 20 °C

5.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran; water / 1 h / 60 - 80 °C

5.2: 20 °C

6.1: lithium hydroxide; water / tetrahydrofuran / 1 h / 20 °C

7.1: n-heptane; isopropyl alcohol / Resolution of racemate

With pyridine; lithium hydroxide; sodium periodate; water; hydrogen; sodium tris(acetoxy)borohydride; sodium carbonate; osmium(VIII) oxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 10 % Pd(OH)2/C; In tetrahydrofuran; ethanol; n-heptane; dichloromethane; water; 1,2-dichloro-ethane; isopropyl alcohol; tert-butyl alcohol;

Reference yield:

: 927803-63-2
4-amino-4,5,6,7-tetrahydro-2H-indazol

: 955407-81-5
C₂₄H₂₂Cl₂FN₃O

: 955407-82-6
C₂₄H₂₂Cl₂FN₃O

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 13 h / 20 - 50 °C

2.1: hydrogen / 10 % Pd(OH)2/C / ethanol / 3 h / 20 °C / 2585.81 Torr

3.1: pyridine / dichloromethane / 0.83 h / 0 - 20 °C

4.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran; water / 1 h / 60 - 80 °C

4.2: 20 °C

5.1: lithium hydroxide; water / tetrahydrofuran / 1 h / 20 °C

6.1: n-heptane; isopropyl alcohol / Resolution of racemate

With pyridine; lithium hydroxide; water; hydrogen; sodium tris(acetoxy)borohydride; sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 10 % Pd(OH)2/C; In tetrahydrofuran; ethanol; n-heptane; dichloromethane; water; 1,2-dichloro-ethane; isopropyl alcohol;