2-(2-chloro-5-((2S,3S,4R,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)tetrahydro-2H-pyran-2-yl)benzyl)-5-(5-phenylfuran-2-yl)-1,3,4-thiadiazole

Base Information

• Chemical Name: 2-(2-chloro-5-((2S,3S,4R,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)tetrahydro-2H-pyran-2-yl)benzyl)-5-(5-phenylfuran-2-yl)-1,3,4-thiadiazole
• CAS No.: 1225430-95-4
• Molecular Formula: C₅₃H₄₇ClN₂O₆S
• Molecular Weight: 875.485

Synonyms:

Chemical Property of 2-(2-chloro-5-((2S,3S,4R,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)tetrahydro-2H-pyran-2-yl)benzyl)-5-(5-phenylfuran-2-yl)-1,3,4-thiadiazole

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 2-(2-chloro-5-((2S,3S,4R,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)tetrahydro-2H-pyran-2-yl)benzyl)-5-(5-phenylfuran-2-yl)-1,3,4-thiadiazole

There total 2 articles about 2-(2-chloro-5-((2S,3S,4R,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)tetrahydro-2H-pyran-2-yl)benzyl)-5-(5-phenylfuran-2-yl)-1,3,4-thiadiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N'-(2-(2-chloro-5-((2S,3S,4R,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)tetrahydro-2H-pyran-2-yl)pgenyl)acetyl)-5-phenylfuran-2-carbohydrazide (1225430-96-5) → 2-(2-chloro-5-((2S,3S,4R,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)tetrahydro-2H-pyran-2-yl)benzyl)-5-(5-phenylfuran-2-yl)-1,3,4-thiadiazole (1225430-95-4)

Guidance literature:

With Lawessons reagent; In tetrahydrofuran; Inert atmosphere; Reflux;

DOI:10.1016/j.bmc.2010.01.073

Reference yield:

→ 2-(2-chloro-5-((2S,3S,4R,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)tetrahydro-2H-pyran-2-yl)benzyl)-5-(5-phenylfuran-2-yl)-1,3,4-thiadiazole (1225430-95-4)

Guidance literature:

Reference yield:

2-(2-chloro-5-((2S,3S,4R,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)tetrahydro-2H-pyran-2-yl)benzyl)-5-(5-phenylfuran-2-yl)-1,3,4-thiadiazole (1225430-95-4) → (2S,3R,4R,5S,6R)-2-(4-chloro-3-((5-(5-phenylfuran-2-yl)-1,3,4-thiadiazol-2-yl)methyl)phenyl)-6-(hydroxymethyl)tetrahydro-2H-pyran-3,4,5-triol (1225430-80-7)

Guidance literature:

With trimethylsilyl iodide; In acetonitrile; at 50 ℃; Inert atmosphere;

DOI:10.1016/j.bmc.2010.01.073

upstream raw materials:

N'-(2-(2-chloro-5-((2S,3S,4R,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)tetrahydro-2H-pyran-2-yl)pgenyl)acetyl)-5-phenylfuran-2-carbohydrazide

Downstream raw materials:

(2S,3R,4R,5S,6R)-2-(4-chloro-3-((5-(5-phenylfuran-2-yl)-1,3,4-thiadiazol-2-yl)methyl)phenyl)-6-(hydroxymethyl)tetrahydro-2H-pyran-3,4,5-triol

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