C₁₄H₅⁽²⁾H₄N₃O₂

Base Information

Chemical Name:C₁₄H₅⁽²⁾H₄N₃O₂
CAS No.:1262802-11-8
Molecular Formula:C₁₄H₉N₃O₂
Molecular Weight:255.213
Hs Code.:

C<sub>14</sub>H<sub>5</sub><sup>(2)</sup>H<sub>4</sub>N<sub>3</sub>O<sub>2</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₄H₅⁽²⁾H₄N₃O₂

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of C₁₄H₅⁽²⁾H₄N₃O₂

There total 8 articles about C₁₄H₅⁽²⁾H₄N₃O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1262802-08-3
2-(phenyl-d₅)quinoxaline

: 5021-43-2
2-phenylquinoxaline

: 1262802-11-8
C₁₄H₅⁽²⁾H₄N₃O₂

: 2-(2-nitrophenyl)-quinoxaline

Guidance literature:: With dipotassium peroxodisulfate; silver(I) nitrite; palladium diacetate; In 1,2-dichloro-ethane; at 130 ℃; for 24h; sealed tube;
DOI:10.1002/chem.201002581

Reference yield:

: 1262802-08-3
2-(phenyl-d₅)quinoxaline

: 1262802-12-9
C₁₄H₆⁽²⁾H₃N₃O₂

: 1262802-11-8
C₁₄H₅⁽²⁾H₄N₃O₂

Guidance literature:: Multi-step reaction with 3 steps

1: [bis(acetoxy)iodo]benzene; palladium diacetate; tetra-(n-butyl)ammonium iodide; acetic acid / 8 h / 120 °C

2: ammonium chloride; zinc / tetrahydrofuran; water / 25 °C

3: silver(I) nitrite; dipotassium peroxodisulfate; palladium diacetate / 1,2-dichloro-ethane / 48 h / 130 °C / sealed tube

With dipotassium peroxodisulfate; silver(I) nitrite; [bis(acetoxy)iodo]benzene; palladium diacetate; tetra-(n-butyl)ammonium iodide; ammonium chloride; acetic acid; zinc; In tetrahydrofuran; water; 1,2-dichloro-ethane;
DOI:10.1002/chem.201002581

Reference yield:

: 28077-64-7
acetophenone-d5

: 1262802-12-9
C₁₄H₆⁽²⁾H₃N₃O₂

: 1262802-11-8
C₁₄H₅⁽²⁾H₄N₃O₂

Guidance literature:: Multi-step reaction with 5 steps

1: tetra-N-butylammonium tribromide / methanol; dichloromethane / 2 h / 30 °C

2: ClHO₄*O₂Si / acetonitrile / 20 °C

3: [bis(acetoxy)iodo]benzene; palladium diacetate; tetra-(n-butyl)ammonium iodide; acetic acid / 8 h / 120 °C

4: ammonium chloride; zinc / tetrahydrofuran; water / 25 °C

5: silver(I) nitrite; dipotassium peroxodisulfate; palladium diacetate / 1,2-dichloro-ethane / 48 h / 130 °C / sealed tube

With dipotassium peroxodisulfate; silver(I) nitrite; [bis(acetoxy)iodo]benzene; ClHO₄*O₂Si; palladium diacetate; tetra-N-butylammonium tribromide; tetra-(n-butyl)ammonium iodide; ammonium chloride; acetic acid; zinc; In tetrahydrofuran; methanol; dichloromethane; water; 1,2-dichloro-ethane; acetonitrile;
DOI:10.1002/chem.201002581