Technology Process of C21H32O6
There total 6 articles about C21H32O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium tetrahydroborate; L-Tartaric acid;
In
tetrahydrofuran;
at -20 ℃;
DOI:10.1021/ol301886g
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: phosphorus tribromide / diethyl ether / 2 h / 0 °C
2.1: sodium hydride; tetra-(n-butyl)ammonium iodide / tetrahydrofuran; mineral oil / 0 - 23 °C / Inert atmosphere
3.1: sodium hydride / tetrahydrofuran / 0.25 h / 0 °C / Inert atmosphere
3.2: Inert atmosphere
4.1: sodium tetrahydroborate; L-Tartaric acid / tetrahydrofuran / -20 °C
With
sodium tetrahydroborate; L-Tartaric acid; phosphorus tribromide; tetra-(n-butyl)ammonium iodide; sodium hydride;
In
tetrahydrofuran; diethyl ether; mineral oil;
DOI:10.1021/ol301886g
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: titanium(IV) isopropylate; L-(+)-diisopropyl tartrate / dichloromethane / 36 h / -40 °C / Inert atmosphere; Molecular sieve
2.1: sodium hydride; tetra-(n-butyl)ammonium iodide / tetrahydrofuran; mineral oil / 0 - 23 °C / Inert atmosphere
3.1: sodium hydride / tetrahydrofuran / 0.25 h / 0 °C / Inert atmosphere
3.2: Inert atmosphere
4.1: sodium tetrahydroborate; L-Tartaric acid / tetrahydrofuran / -20 °C
With
titanium(IV) isopropylate; sodium tetrahydroborate; L-Tartaric acid; L-(+)-diisopropyl tartrate; tetra-(n-butyl)ammonium iodide; sodium hydride;
In
tetrahydrofuran; dichloromethane; mineral oil;
DOI:10.1021/ol301886g
