C₁₅H₂₄O₂Si

Base Information

• Chemical Name: C₁₅H₂₄O₂Si
• CAS No.: 1355253-97-2
• Molecular Formula: C₁₅H₂₄O₂Si
• Molecular Weight: 264.44
• Mol file: 1355253-97-2.mol

Synonyms:

Chemical Property of C₁₅H₂₄O₂Si

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of C₁₅H₂₄O₂Si

There total 1 articles about C₁₅H₂₄O₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(3-methoxyphenyl)-2-methyl-propan-1-one (6026-75-1) → C15H24O2Si (1355253-97-2)

Guidance literature:

Multi-step reaction with 2 steps

1.1: n-butyllithium; diisopropylamine / tetrahydrofuran; hexane / 1 h / 0 °C / Inert atmosphere

1.2: Inert atmosphere

2.1: diethylzinc / dichloromethane / 16 h / 0 °C / Inert atmosphere

With n-butyllithium; diethylzinc; diisopropylamine; In tetrahydrofuran; hexane; dichloromethane;

DOI:10.1039/c2cc16758a

Reference yield: 70.0%

C15H24O2Si (1355253-97-2) → 6-methoxy-2,2-dimethyl-1-indanone (124688-07-9)

Guidance literature:

C₁₅H₂₄O₂Si; With potassium acetate; palladium diacetate; In N,N-dimethyl acetamide; at 20 ℃; for 0.0833333h; Inert atmosphere;

With tetrabutyl ammonium fluoride; oxygen; In N,N-dimethyl acetamide; at 20 - 100 ℃;

DOI:10.1039/c2cc16758a

upstream raw materials:

1-(3-methoxyphenyl)-2-methyl-propan-1-one

Downstream raw materials:

6-methoxy-2,2-dimethyl-1-indanone

Refernces