C₂₅H₂₂BrF₄N₃O₃

Base Information

Chemical Name:C₂₅H₂₂BrF₄N₃O₃
CAS No.:1617505-11-9
Molecular Formula:C₂₅H₂₂BrF₄N₃O₃
Molecular Weight:568.366
Hs Code.:

C<sub>25</sub>H<sub>22</sub>BrF<sub>4</sub>N<sub>3</sub>O<sub>3</sub>

Synonyms:

Suppliers and Price of C₂₅H₂₂BrF₄N₃O₃

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₂₅H₂₂BrF₄N₃O₃

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₅H₂₂BrF₄N₃O₃

There total 5 articles about C₂₅H₂₂BrF₄N₃O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1555701-66-0
4-bromo-6-fluoro-7-methoxy-3,3-dimethyl-1-(2-nitrophenyl)indoline

: 1617505-11-9
C₂₅H₂₂BrF₄N₃O₃

Guidance literature:: Multi-step reaction with 2 steps

1: zinc; ammonium chloride / methanol; ethyl acetate / 20 °C / Inert atmosphere

2: dichloromethane / 16 h / 20 °C / Inert atmosphere

With ammonium chloride; zinc; In methanol; dichloromethane; ethyl acetate;
DOI:10.1021/jm5006226

Reference yield:

: 239122-51-1
5-bromo-3-fluoro-2-methoxyaniline

: 1617505-11-9
C₂₅H₂₂BrF₄N₃O₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: hydrogenchloride; sodium nitrite / water / -10 °C / Inert atmosphere

2.1: dichloromethane / 20 °C / Inert atmosphere

2.2: 2 h / Inert atmosphere

2.3: 0.17 h / 0 °C / Inert atmosphere

3.1: 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; caesium carbonate / toluene / Inert atmosphere; Sealed tube

4.1: zinc; ammonium chloride / methanol; ethyl acetate / 20 °C / Inert atmosphere

5.1: dichloromethane / 16 h / 20 °C / Inert atmosphere

With hydrogenchloride; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; ammonium chloride; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; zinc; sodium nitrite; In methanol; dichloromethane; water; ethyl acetate; toluene; 2.1: |Fischer Indole Synthesis;
DOI:10.1021/jm5006226

Reference yield:

: 1379365-84-0
C₇H₈BrFN₂O

: 1617505-11-9
C₂₅H₂₂BrF₄N₃O₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: dichloromethane / 20 °C / Inert atmosphere

1.2: 2 h / Inert atmosphere

1.3: 0.17 h / 0 °C / Inert atmosphere

2.1: 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; caesium carbonate / toluene / Inert atmosphere; Sealed tube

3.1: zinc; ammonium chloride / methanol; ethyl acetate / 20 °C / Inert atmosphere

4.1: dichloromethane / 16 h / 20 °C / Inert atmosphere

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; ammonium chloride; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; zinc; In methanol; dichloromethane; ethyl acetate; toluene; 1.1: |Fischer Indole Synthesis;
DOI:10.1021/jm5006226