C₄₈H₆₇N₉O₁₃S₂

Base Information

Chemical Name:C₄₈H₆₇N₉O₁₃S₂
CAS No.:1147996-32-4
Molecular Formula:C₄₈H₆₇N₉O₁₃S₂
Molecular Weight:1042.24
Hs Code.:

C<sub>48</sub>H<sub>67</sub>N<sub>9</sub>O<sub>13</sub>S<sub>2</sub>

Synonyms:

Suppliers and Price of C₄₈H₆₇N₉O₁₃S₂

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₄₈H₆₇N₉O₁₃S₂

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₄₈H₆₇N₉O₁₃S₂

There total 7 articles about C₄₈H₆₇N₉O₁₃S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1147996-34-6
Fmoc-Ile-Ser(Ψ^Me,MePro)-OH

: 1147996-32-4
C₄₈H₆₇N₉O₁₃S₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: piperidine; 1,8-diazabicyclo[5.4.0]undec-7-ene / N,N-dimethyl-formamide / Automated synthesizer; solid phase reaction

1.2: Automated synthesizer; solid phase reaction

2.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 3-hydroxy-3,4-dihydrobenzotriazine-4-one / chloroform; 2,2,2-trifluoroethanol / 2.5 h / Inert atmosphere

3.1: chlorotriisopropylsilane; water; trifluoroacetic acid; phenol / 2 h / Inert atmosphere

With piperidine; chlorotriisopropylsilane; water; 1,8-diazabicyclo[5.4.0]undec-7-ene; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 3-hydroxy-3,4-dihydrobenzotriazine-4-one; trifluoroacetic acid; phenol; In chloroform; 2,2,2-trifluoroethanol; N,N-dimethyl-formamide;
DOI:10.1002/anie.201107482

Reference yield:

: 1360878-92-7
C₂₂H₂₄N₂O₃S

: 1147996-32-4
C₄₈H₆₇N₉O₁₃S₂

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride / 1,4-dioxane / 1 h / 20 °C / Inert atmosphere

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 3-hydroxy-3,4-dihydrobenzotriazine-4-one / chloroform; 2,2,2-trifluoroethanol / 2.5 h / Inert atmosphere

3: chlorotriisopropylsilane; water; trifluoroacetic acid; phenol / 2 h / Inert atmosphere

With hydrogenchloride; chlorotriisopropylsilane; water; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 3-hydroxy-3,4-dihydrobenzotriazine-4-one; trifluoroacetic acid; phenol; In 1,4-dioxane; chloroform; 2,2,2-trifluoroethanol;
DOI:10.1002/anie.201107482

Reference yield:

: 108-98-5
thiophenol

: 1147996-32-4
C₄₈H₆₇N₉O₁₃S₂

Guidance literature:: Multi-step reaction with 4 steps

1: dicyclohexyl-carbodiimide / ethyl acetate / 1.5 h / 0 - 20 °C / Inert atmosphere

2: hydrogenchloride / 1,4-dioxane / 1 h / 20 °C / Inert atmosphere

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 3-hydroxy-3,4-dihydrobenzotriazine-4-one / chloroform; 2,2,2-trifluoroethanol / 2.5 h / Inert atmosphere

4: chlorotriisopropylsilane; water; trifluoroacetic acid; phenol / 2 h / Inert atmosphere

With hydrogenchloride; chlorotriisopropylsilane; water; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 3-hydroxy-3,4-dihydrobenzotriazine-4-one; dicyclohexyl-carbodiimide; trifluoroacetic acid; phenol; In 1,4-dioxane; chloroform; 2,2,2-trifluoroethanol; ethyl acetate;
DOI:10.1002/anie.201107482