6-cyclohexyl-11H-benzo[a]naphtho[2,1-c]carbazole

Base Information

Chemical Name:6-cyclohexyl-11H-benzo[a]naphtho[2,1-c]carbazole
CAS No.:1337901-70-8
Molecular Formula:C₃₀H₂₅N
Molecular Weight:399.535
Hs Code.:

Synonyms:

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Chemical Property of 6-cyclohexyl-11H-benzo[a]naphtho[2,1-c]carbazole

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Technology Process of 6-cyclohexyl-11H-benzo[a]naphtho[2,1-c]carbazole

There total 4 articles about 6-cyclohexyl-11H-benzo[a]naphtho[2,1-c]carbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1337901-51-5
2-[(2-{[2-(cyclohexylethynyl)phenyl]ethynyl}phenyl)ethynyl]aniline

: 1337901-70-8
6-cyclohexyl-11H-benzo[a]naphtho[2,1-c]carbazole

Guidance literature:: With silver tetrafluoroborate; 2-(di-tert-butylphosphino)-1,1'-biphenylgold(I) chloride; acetic acid; at 80 ℃; for 24h; Inert atmosphere;
DOI:10.1021/jo2018119

Reference yield:

: 852619-15-9
2-({2-[(trimethylsilyl)ethynyl]phenyl}ethynyl)aniline

: 1337901-70-8
6-cyclohexyl-11H-benzo[a]naphtho[2,1-c]carbazole

Guidance literature:: Multi-step reaction with 3 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 °C

2: copper(l) iodide; bis(benzonitrile)palladium(II) dichloride; tri-tert-butyl phosphine; diisopropylamine / tetrahydrofuran / 10 h / 20 °C / Inert atmosphere

3: silver tetrafluoroborate; 2-(di-tert-butylphosphino)-1,1'-biphenylgold(I) chloride; acetic acid / 24 h / 80 °C / Inert atmosphere

With copper(l) iodide; bis(benzonitrile)palladium(II) dichloride; silver tetrafluoroborate; 2-(di-tert-butylphosphino)-1,1'-biphenylgold(I) chloride; tri-tert-butyl phosphine; tetrabutyl ammonium fluoride; acetic acid; diisopropylamine; In tetrahydrofuran; 2: Sonogashira coupling;
DOI:10.1021/jo2018119

Reference yield:

: 1224635-50-0
2-[(2-ethynylphenyl)ethynyl]aniline

: 1337901-70-8
6-cyclohexyl-11H-benzo[a]naphtho[2,1-c]carbazole

Guidance literature:: Multi-step reaction with 2 steps

1: copper(l) iodide; bis(benzonitrile)palladium(II) dichloride; tri-tert-butyl phosphine; diisopropylamine / tetrahydrofuran / 10 h / 20 °C / Inert atmosphere

2: silver tetrafluoroborate; 2-(di-tert-butylphosphino)-1,1'-biphenylgold(I) chloride; acetic acid / 24 h / 80 °C / Inert atmosphere

With copper(l) iodide; bis(benzonitrile)palladium(II) dichloride; silver tetrafluoroborate; 2-(di-tert-butylphosphino)-1,1'-biphenylgold(I) chloride; tri-tert-butyl phosphine; acetic acid; diisopropylamine; In tetrahydrofuran; 1: Sonogashira coupling;
DOI:10.1021/jo2018119