C₂₁H₂₁NO₅

Base Information

Chemical Name:C₂₁H₂₁NO₅
CAS No.:1394849-50-3
Molecular Formula:C₂₁H₂₁NO₅
Molecular Weight:367.401
Hs Code.:

C<sub>21</sub>H<sub>21</sub>NO<sub>5</sub>

Synonyms:

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Chemical Property of C₂₁H₂₁NO₅

Chemical Property:

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Technology Process of C₂₁H₂₁NO₅

There total 4 articles about C₂₁H₂₁NO₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 117087-17-9
5-[(benzyloxy)methyl]-2,2-dimethyl-1,3-dioxane

: 1394849-50-3
C₂₁H₂₁NO₅

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogenchloride / water; isopropyl alcohol / 3 h / 25 °C / Large scale

2: Lipase AS Amano from (Aspergillus niger) / dimethyl sulfoxide / 20 h / 37 °C / pH 7.5 / Enzymatic reaction

3: triethylamine / toluene / 1 h / -5 - 0 °C / Acidic conditions

4: N,N-dimethyl-formamide

With hydrogenchloride; Lipase AS Amano from (Aspergillus niger); triethylamine; In water; dimethyl sulfoxide; N,N-dimethyl-formamide; isopropyl alcohol; toluene; 4: |Gabriel Amine Synthesis;
DOI:10.1021/op3001383

Reference yield:

: 117087-18-0
2-((benzyloxy)methyl)propane-1,3-diol

: 1394849-50-3
C₂₁H₂₁NO₅

Guidance literature:: Multi-step reaction with 3 steps

1: Lipase AS Amano from (Aspergillus niger) / dimethyl sulfoxide / 20 h / 37 °C / pH 7.5 / Enzymatic reaction

2: triethylamine / toluene / 1 h / -5 - 0 °C / Acidic conditions

3: N,N-dimethyl-formamide

With Lipase AS Amano from (Aspergillus niger); triethylamine; In dimethyl sulfoxide; N,N-dimethyl-formamide; toluene; 3: |Gabriel Amine Synthesis;
DOI:10.1021/op3001383

Reference yield:

: 100-39-0
benzyl bromide

: 1394849-50-3
C₂₁H₂₁NO₅

Guidance literature:: Multi-step reaction with 5 steps

1: potassium hydroxide; tetrabutylammomium bromide / toluene; water / 10 h / 25 - 50 °C

2: hydrogenchloride / water; isopropyl alcohol / 3 h / 25 °C / Large scale

3: Lipase AS Amano from (Aspergillus niger) / dimethyl sulfoxide / 20 h / 37 °C / pH 7.5 / Enzymatic reaction

4: triethylamine / toluene / 1 h / -5 - 0 °C / Acidic conditions

5: N,N-dimethyl-formamide

With hydrogenchloride; Lipase AS Amano from (Aspergillus niger); tetrabutylammomium bromide; triethylamine; potassium hydroxide; In water; dimethyl sulfoxide; N,N-dimethyl-formamide; isopropyl alcohol; toluene; 5: |Gabriel Amine Synthesis;
DOI:10.1021/op3001383