Technology Process of C62H67F3IN10O6(1+)
There total 4 articles about C62H67F3IN10O6(1+) which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: rhodium(II) acetate dimer / dichloromethane / 10 h / Inert atmosphere
2: diisobutylaluminium hydride / toluene / 1 h / -78 °C / Inert atmosphere
3: water; dimethyl sulfoxide
With
rhodium(II) acetate dimer; diisobutylaluminium hydride;
In
dichloromethane; water; dimethyl sulfoxide; toluene;
DOI:10.1021/ja502780z
- Guidance literature:
-
Multi-step reaction with 2 steps
1: diisobutylaluminium hydride / toluene / 1 h / -78 °C / Inert atmosphere
2: water; dimethyl sulfoxide
With
diisobutylaluminium hydride;
In
water; dimethyl sulfoxide; toluene;
DOI:10.1021/ja502780z
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: trifluoroacetic acid / dichloromethane / 8 h / 20 °C / Inert atmosphere
1.2: 20 °C / Inert atmosphere
2.1: water; dimethyl sulfoxide
With
trifluoroacetic acid;
In
dichloromethane; water; dimethyl sulfoxide;
DOI:10.1021/ja502780z