6,6'-Dimethyl-4,4'-diphenyl-2H,2'H-[1,1'-bipyrimidine]-2,2'-dione

Base Information

Chemical Name:6,6'-Dimethyl-4,4'-diphenyl-2H,2'H-[1,1'-bipyrimidine]-2,2'-dione
CAS No.:105686-94-0
Molecular Formula:C22H18N4O2
Molecular Weight:370.411
Hs Code.:
DSSTox Substance ID:DTXSID30542706
Wikidata:Q82419446

Synonyms:105686-94-0;DTXSID30542706;6,6'-Dimethyl-4,4'-diphenyl-2H,2'H-[1,1'-bipyrimidine]-2,2'-dione

Suppliers and Price of 6,6'-Dimethyl-4,4'-diphenyl-2H,2'H-[1,1'-bipyrimidine]-2,2'-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6,6'-Dimethyl-4,4'-diphenyl-2H,2'H-[1,1'-bipyrimidine]-2,2'-dione

Chemical Property:

XLogP3:3.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:370.14297583
Heavy Atom Count:28
Complexity:714

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=NC(=O)N1N2C(=CC(=NC2=O)C3=CC=CC=C3)C)C4=CC=CC=C4

Technology Process of 6,6'-Dimethyl-4,4'-diphenyl-2H,2'H-[1,1'-bipyrimidine]-2,2'-dione

There total 2 articles about 6,6'-Dimethyl-4,4'-diphenyl-2H,2'H-[1,1'-bipyrimidine]-2,2'-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 105701-02-8
[(Z)-3-(N'-{(Z)-3-[(E)-Ethoxycarbonylimino]-1-methyl-3-phenyl-propenyl}-hydrazino)-1-phenyl-but-2-en-(E)-ylidene]-carbamic acid ethyl ester

: 105686-94-0
6,6'-Dimethyl-4,4'-diphenyl-[1,1']bipyrimidinyl-2,2'-dione

Guidance literature:: With n-butyllithium; In tetrahydrofuran; for 20h; Ambient temperature;
DOI:10.1055/s-1985-31456

Reference yield:

: 105687-00-1
(Z)-3-[N'-((Z)-3-Imino-1-methyl-3-phenyl-propenyl)-hydrazino]-1-phenyl-but-2-enylideneamine

: 105686-94-0
6,6'-Dimethyl-4,4'-diphenyl-[1,1']bipyrimidinyl-2,2'-dione

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / pyridine / 5 h / 60 °C

2: 78 percent / n-C₄H₉Li / tetrahydrofuran / 20 h / Ambient temperature

With n-butyllithium; In tetrahydrofuran; pyridine;
DOI:10.1055/s-1985-31456