13-Oxa-2,6,7,11-tetraazapentadeca-2,4,8,10-tetraenoic acid, 5,8-dimethyl-12-oxo-3,10-diphenyl-, ethyl ester, (Z,Z,E,E)-

Base Information

• Chemical Name: 13-Oxa-2,6,7,11-tetraazapentadeca-2,4,8,10-tetraenoic acid, 5,8-dimethyl-12-oxo-3,10-diphenyl-, ethyl ester, (Z,Z,E,E)-
• CAS No.: 105701-02-8
• Molecular Formula: C26H30N4O4
• Molecular Weight: 462.549
• Mol file: 105701-02-8.mol

Synonyms:

Chemical Property of 13-Oxa-2,6,7,11-tetraazapentadeca-2,4,8,10-tetraenoic acid, 5,8-dimethyl-12-oxo-3,10-diphenyl-, ethyl ester, (Z,Z,E,E)-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 13-Oxa-2,6,7,11-tetraazapentadeca-2,4,8,10-tetraenoic acid, 5,8-dimethyl-12-oxo-3,10-diphenyl-, ethyl ester, (Z,Z,E,E)-

There total 1 articles about 13-Oxa-2,6,7,11-tetraazapentadeca-2,4,8,10-tetraenoic acid, 5,8-dimethyl-12-oxo-3,10-diphenyl-, ethyl ester, (Z,Z,E,E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

chloroformic acid ethyl ester (541-41-3) + (Z)-3-[N'-((Z)-3-Imino-1-methyl-3-phenyl-propenyl)-hydrazino]-1-phenyl-but-2-enylideneamine (105687-00-1) → [(Z)-3-(N'-{(Z)-3-[(E)-Ethoxycarbonylimino]-1-methyl-3-phenyl-propenyl}-hydrazino)-1-phenyl-but-2-en-(E)-ylidene]-carbamic acid ethyl ester (105701-02-8)

Guidance literature:

In pyridine; at 60 ℃; for 5h;

DOI:10.1055/s-1985-31456

Reference yield: 78.0%

[(Z)-3-(N'-{(Z)-3-[(E)-Ethoxycarbonylimino]-1-methyl-3-phenyl-propenyl}-hydrazino)-1-phenyl-but-2-en-(E)-ylidene]-carbamic acid ethyl ester (105701-02-8) → 6,6'-Dimethyl-4,4'-diphenyl-[1,1']bipyrimidinyl-2,2'-dione (105686-94-0)

Guidance literature:

With n-butyllithium; In tetrahydrofuran; for 20h; Ambient temperature;

DOI:10.1055/s-1985-31456

upstream raw materials:

chloroformic acid ethyl ester

(Z)-3-[N'-((Z)-3-Imino-1-methyl-3-phenyl-propenyl)-hydrazino]-1-phenyl-but-2-enylideneamine

Downstream raw materials:

6,6'-Dimethyl-4,4'-diphenyl-[1,1']bipyrimidinyl-2,2'-dione

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