C₃₉H₅₇NO₅Si

Base Information

Chemical Name:C₃₉H₅₇NO₅Si
CAS No.:124692-03-1
Molecular Formula:C₃₉H₅₇NO₅Si
Molecular Weight:647.971
Hs Code.:

C<sub>39</sub>H<sub>57</sub>NO<sub>5</sub>Si

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₉H₅₇NO₅Si

Chemical Property:

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Technology Process of C₃₉H₅₇NO₅Si

There total 15 articles about C₃₉H₅₇NO₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 2186-92-7
p-Anisaldehyde dimethyl acetal

: 118378-08-8,124815-81-2
C₃₁H₅₁NO₄Si

: 124692-03-1
C₃₉H₅₇NO₅Si

Guidance literature:: With pyridinium p-toluenesulfonate; In N,N-dimethyl-formamide; for 1.5h; Ambient temperature;
DOI:10.1016/S0040-4020(01)83440-2

Reference yield:

: 124665-33-4
(1R,2S,6S,7S)-2-Benzyloxymethyl-5-oxo-bicyclo[4.2.0]octane-7-carboxylic acid methyl ester

: 124692-03-1
C₃₉H₅₇NO₅Si

Guidance literature:: Multi-step reaction with 15 steps

1: amberlyst 15 / 2 h / 0 °C

2: benzene; diethyl ether / 0.58 h

3: pyridinium p-toluenesulfonate / acetone / 0.33 h / Ambient temperature

4: 84 percent / N-ethyldiisopropylamine / CH₂Cl₂ / 46 h / Ambient temperature

5: sodium hydride / tetrahydrofuran / 6.5 h / Ambient temperature

6: triethylamine / 1.) 0 deg C, 1h; 2.) rt, 36h

7: potassium hydroxide / methanol; H₂O / 2.5 h / Heating

8: 87 percent / hydroxylamine hydrochloride, sodium acetate / methanol / 0.67 h / Heating

9: xylene / 0.83 h / 150 °C

10: sodium hydroxide / ethanol; H₂O / 7.25 h / Heating

11: 84 percent / H₂, (1S)-(+)-10-camphorsulfonic acid / palladium hydroxide on carbon / ethyl acetate / 22.5 h

12: 85 percent / N-ethyldiisopropylamine / 4-dimethylaminopyridine / CH₂Cl₂ / 1.) 0 deg C, 40 min; 2.) rt,1.33 h

13: lithium diisopropylamide / hexane; tetrahydrofuran / 1.) 0 deg C, 50 min; 2.) rt, 50 min

14: 83 percent / n-BuLi / hexane; tetrahydrofuran / 1.1 h / Ambient temperature

15: 35 percent / pyridinium p-toluenesulfonate / dimethylformamide / 1.5 h / Ambient temperature

With potassium hydroxide; sodium hydroxide; n-butyllithium; Amberlyst 15; hydroxylamine hydrochloride; hydrogen; sodium acetate; pyridinium p-toluenesulfonate; sodium hydride; (+)-10-camphorsulfonic acid; triethylamine; N-ethyl-N,N-diisopropylamine; lithium diisopropyl amide; dmap; palladium dihydroxide; In tetrahydrofuran; methanol; diethyl ether; ethanol; hexane; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; acetone; xylene; benzene;
DOI:10.1016/S0040-4020(01)83440-2

Reference yield:

: 118378-03-3
(1S,5S,6R,8S)-5-Benzyloxymethyl-8-(1-hydroxy-1-methyl-ethyl)-bicyclo[4.2.0]octan-2-one

: 124692-03-1
C₃₉H₅₇NO₅Si

Guidance literature:: Multi-step reaction with 12 steps

1: 84 percent / N-ethyldiisopropylamine / CH₂Cl₂ / 46 h / Ambient temperature

2: sodium hydride / tetrahydrofuran / 6.5 h / Ambient temperature

3: triethylamine / 1.) 0 deg C, 1h; 2.) rt, 36h

4: potassium hydroxide / methanol; H₂O / 2.5 h / Heating

5: 87 percent / hydroxylamine hydrochloride, sodium acetate / methanol / 0.67 h / Heating

6: xylene / 0.83 h / 150 °C

7: sodium hydroxide / ethanol; H₂O / 7.25 h / Heating

8: 84 percent / H₂, (1S)-(+)-10-camphorsulfonic acid / palladium hydroxide on carbon / ethyl acetate / 22.5 h

9: 85 percent / N-ethyldiisopropylamine / 4-dimethylaminopyridine / CH₂Cl₂ / 1.) 0 deg C, 40 min; 2.) rt,1.33 h

10: lithium diisopropylamide / hexane; tetrahydrofuran / 1.) 0 deg C, 50 min; 2.) rt, 50 min

11: 83 percent / n-BuLi / hexane; tetrahydrofuran / 1.1 h / Ambient temperature

12: 35 percent / pyridinium p-toluenesulfonate / dimethylformamide / 1.5 h / Ambient temperature

With potassium hydroxide; sodium hydroxide; n-butyllithium; hydroxylamine hydrochloride; hydrogen; sodium acetate; pyridinium p-toluenesulfonate; sodium hydride; (+)-10-camphorsulfonic acid; triethylamine; N-ethyl-N,N-diisopropylamine; lithium diisopropyl amide; dmap; palladium dihydroxide; In tetrahydrofuran; methanol; ethanol; hexane; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; xylene;
DOI:10.1016/S0040-4020(01)83440-2