C₁₄H₁₆FN₃O

Base Information

Chemical Name:C₁₄H₁₆FN₃O
CAS No.:1404115-67-8
Molecular Formula:C₁₄H₁₆FN₃O
Molecular Weight:261.299
Hs Code.:

C<sub>14</sub>H<sub>16</sub>FN<sub>3</sub>O

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₄H₁₆FN₃O

Chemical Property:

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Technology Process of C₁₄H₁₆FN₃O

There total 5 articles about C₁₄H₁₆FN₃O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1375069-06-9
(2-bromo-6-fluoro-3-methylphenyl)methanol

: 1404115-67-8
C₁₄H₁₆FN₃O

Guidance literature:: Multi-step reaction with 7 steps

1: thionyl chloride / tetrahydrofuran

2: triethylamine / dimethyl sulfoxide

3: borane-THF / tetrahydrofuran

4: sodium hydroxide / tetrahydrofuran; water

5: potassium acetate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,4-dioxane / Heating

6: potassium carbonate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / isopropyl alcohol / Heating

7: trifluoroacetic acid / dichloromethane

With thionyl chloride; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; borane-THF; potassium acetate; potassium carbonate; triethylamine; trifluoroacetic acid; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; dimethyl sulfoxide; isopropyl alcohol; 5: |Suzuki Coupling / 6: |Suzuki Coupling;
DOI:10.1016/j.bmcl.2012.08.031

Reference yield:

: C₂₀H₃₁BFNO₄

: 1404115-67-8
C₁₄H₁₆FN₃O

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / isopropyl alcohol / Heating

2: trifluoroacetic acid / dichloromethane

With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium carbonate; trifluoroacetic acid; In dichloromethane; isopropyl alcohol; 1: |Suzuki Coupling;
DOI:10.1016/j.bmcl.2012.08.031