Toluene-4-sulfonate(2-ethoxycarbonyl-ethyl)-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-2-hydroxy-decyl)-dimethyl-ammonium;

Base Information

Chemical Name:Toluene-4-sulfonate(2-ethoxycarbonyl-ethyl)-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-2-hydroxy-decyl)-dimethyl-ammonium;
CAS No.:145398-27-2
Molecular Formula:C₇H₇O₃S*C₁₇H₁₉F₁₇NO₃
Molecular Weight:779.512
Hs Code.:

Synonyms:

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Chemical Property of Toluene-4-sulfonate(2-ethoxycarbonyl-ethyl)-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-2-hydroxy-decyl)-dimethyl-ammonium;

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Technology Process of Toluene-4-sulfonate(2-ethoxycarbonyl-ethyl)-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-2-hydroxy-decyl)-dimethyl-ammonium;

There total 3 articles about Toluene-4-sulfonate(2-ethoxycarbonyl-ethyl)-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-2-hydroxy-decyl)-dimethyl-ammonium; which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 20120-21-2
ethyl 3-(N,N-dimethylamino)propionate

: 135462-67-8
Toluene-4-sulfonic acid 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-2-hydroxy-decyl ester

: 145398-27-2
Toluene-4-sulfonate(2-ethoxycarbonyl-ethyl)-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-2-hydroxy-decyl)-dimethyl-ammonium;

Guidance literature:: In ethanol; at 60 ℃; for 48h;

Reference yield:

: 55118-40-6
1H,1H,2H-perfluorodecane-1,2-diol

: 145398-27-2
Toluene-4-sulfonate(2-ethoxycarbonyl-ethyl)-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-2-hydroxy-decyl)-dimethyl-ammonium;

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / pyridine / diethyl ether / 1) 0 deg C, 2 h, 2) 40 deg C, 72 h

2: 71 percent / ethanol / 48 h / 60 °C

With pyridine; In diethyl ether; ethanol;

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 145398-27-2
Toluene-4-sulfonate(2-ethoxycarbonyl-ethyl)-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-2-hydroxy-decyl)-dimethyl-ammonium;

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / pyridine / diethyl ether / 1) 0 deg C, 2 h, 2) 40 deg C, 72 h

2: 71 percent / ethanol / 48 h / 60 °C

With pyridine; In diethyl ether; ethanol;