Toluene-4-sulfonic acid 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-2-hydroxy-decyl ester

Base Information

• Chemical Name: Toluene-4-sulfonic acid 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-2-hydroxy-decyl ester
• CAS No.: 135462-67-8
• Molecular Formula: C₁₇H₁₁F₁₇O₄S
• Molecular Weight: 634.311

Synonyms:Toluene-4-sulfonic acid 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-2-hydroxy-decyl ester

Chemical Property of Toluene-4-sulfonic acid 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-2-hydroxy-decyl ester

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Technology Process of Toluene-4-sulfonic acid 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-2-hydroxy-decyl ester

There total 1 articles about Toluene-4-sulfonic acid 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-2-hydroxy-decyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

1H,1H,2H-perfluorodecane-1,2-diol (55118-40-6) + p-toluenesulfonyl chloride (98-59-9) → Toluene-4-sulfonic acid 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-2-hydroxy-decyl ester (135462-67-8)

Guidance literature:

With pyridine; In diethyl ether; at 40 ℃; for 72h;

DOI:10.1080/00397919108019752

Reference yield: 82.0%

Toluene-4-sulfonic acid 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-2-hydroxy-decyl ester (135462-67-8) + 2,2'-iminobis[ethanol] (111-42-2) → 1-[Bis-(2-hydroxy-ethyl)-amino]-3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decan-2-ol; compound with toluene-4-sulfonic acid (145398-23-8)

Guidance literature:

In ethanol; at 60 ℃; for 48h;

Reference yield: 78.0%

N,N'-dimethylbenzylamine (103-83-3) + Toluene-4-sulfonic acid 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-2-hydroxy-decyl ester (135462-67-8) → Toluene-4-sulfonatebenzyl-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-2-hydroxy-decyl)-dimethyl-ammonium; (145398-29-4)

Guidance literature:

In ethanol; at 60 ℃; for 48h;

upstream raw materials:

1H,1H,2H-perfluorodecane-1,2-diol

p-toluenesulfonyl chloride

Downstream raw materials:

Toluene-4-sulfonatebenzyl-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-2-hydroxy-decyl)-dimethyl-ammonium;

Toluene-4-sulfonate(2-ethoxycarbonyl-ethyl)-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-2-hydroxy-decyl)-dimethyl-ammonium;

1-[Bis-(2-hydroxy-ethyl)-amino]-3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decan-2-ol; compound with toluene-4-sulfonic acid

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