(m-chloroaniline(-2H))14Ta₆O

Base Information

Chemical Name:(m-chloroaniline(-2H))14Ta₆O
CAS No.:928761-54-0
Molecular Formula:C₈₄H₅₆Cl₁₄N₁₄OTa₆
Molecular Weight:2859.49
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (m-chloroaniline(-2H))14Ta₆O

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Technology Process of (m-chloroaniline(-2H))14Ta₆O

There total 2 articles about (m-chloroaniline(-2H))14Ta₆O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

: [Ta(benzyl)3(N(tert-butyl))]

: 108-42-9
3-chloro-aniline

: 1006689-81-1,928761-54-0
(m-chloroaniline(-2H))14Ta₆O

Guidance literature:: In hexane; benzene; m-chloroaniline (0.950 mmol) treated with degassed water (0.03 mmol), dissolved in C6H6, added to soln. of (C6H5CH2)3TaNC(CH3)3 (0.190 mmol) (benzene), hexane added, mixt. heated at 135°C for 24 h in sealed vessel, cooled to room temp.; solvent removed (under vac.), dissolved in toluene, pentane allowed to diffuse, elem. anal.;
DOI:10.1002/anie.200603019

Reference yield: 15.0%

: [Ta(benzyl)3(N(tert-butyl))]

: 7732-18-5
water

: 108-42-9
3-chloro-aniline

: 1006689-81-1,928761-54-0
(m-chloroaniline(-2H))14Ta₆O

Guidance literature:: In hexane; benzene; (N2); a C6H6 soln. of Ta compd. and a C6H6 soln. of ligand and H2O mixed, hexane added, sealed, heated for ca 24 h at 135°C; allowed to cool, evapd. (vac.), dissolved in toluene, crystd. by pentanediffusion; elem. anal.;
DOI:10.1021/ic701920v