1-<2-ethyl>-1,2,5,6-tetrahydro-3-pyridinecarboxylic acid

Base Information

Chemical Name:1-<2-ethyl>-1,2,5,6-tetrahydro-3-pyridinecarboxylic acid
CAS No.:143747-64-2
Molecular Formula:C₂₁H₂₁Cl₂NO₃
Molecular Weight:406.309
Hs Code.:

1-<2-<bis(4-chlorophenyl)methoxy>ethyl>-1,2,5,6-tetrahydro-3-pyridinecarboxylic acid

Synonyms:

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Chemical Property of 1-<2-ethyl>-1,2,5,6-tetrahydro-3-pyridinecarboxylic acid

Chemical Property:

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Technology Process of 1-<2-ethyl>-1,2,5,6-tetrahydro-3-pyridinecarboxylic acid

There total 4 articles about 1-<2-ethyl>-1,2,5,6-tetrahydro-3-pyridinecarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 128173-97-7
1-<2-ethyl>-1,2,5,6-tetrahydro-3-pyridinecarboxylic acid methyl ester

: 143747-64-2
1-<2-ethyl>-1,2,5,6-tetrahydro-3-pyridinecarboxylic acid

Guidance literature:: With lithium hydroxide; In methanol; for 64h; Ambient temperature;
DOI:10.1021/jm00100a032

Reference yield:

: 495-19-2
norarecoline

: 143747-64-2
1-<2-ethyl>-1,2,5,6-tetrahydro-3-pyridinecarboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: K₂CO₃ / acetonitrile / 15 h / Heating

2: 2 N aq. LiOH / methanol / 64 h / Ambient temperature

With lithium hydroxide; potassium carbonate; In methanol; acetonitrile;
DOI:10.1021/jm00100a032

Reference yield:

: 90-97-1
4,4'-dichlorobenzophenone

: 143747-64-2
1-<2-ethyl>-1,2,5,6-tetrahydro-3-pyridinecarboxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1: conc. H₂SO₄ / toluene / 2 h / 85 - 90 °C

2: K₂CO₃ / acetonitrile / 15 h / Heating

3: 2 N aq. LiOH / methanol / 64 h / Ambient temperature

With lithium hydroxide; sulfuric acid; potassium carbonate; In methanol; toluene; acetonitrile;
DOI:10.1021/jm00100a032