C₃₂H₂₇F₃N₆O₄

Base Information

Chemical Name:C₃₂H₂₇F₃N₆O₄
CAS No.:1031860-39-5
Molecular Formula:C₃₂H₂₇F₃N₆O₄
Molecular Weight:616.599
Hs Code.:

C<sub>32</sub>H<sub>27</sub>F<sub>3</sub>N<sub>6</sub>O<sub>4</sub>

Synonyms:

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Chemical Property of C₃₂H₂₇F₃N₆O₄

Chemical Property:

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Technology Process of C₃₂H₂₇F₃N₆O₄

There total 11 articles about C₃₂H₂₇F₃N₆O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 364-76-1
4-Fluoro-3-nitroaniline

: 1031860-39-5
C₃₂H₂₇F₃N₆O₄

Guidance literature:: Multi-step reaction with 7 steps

1: sodium nitrite; hydrogenchloride; tin(ll) chloride / water / -25 - 20 °C

2: acetic acid

3: triethylamine / tetrahydrofuran

4: hydrogenchloride; tin / tetrahydrofuran; water

5: potassium peroxymonosulfate / water; N,N-dimethyl-formamide

6: acetic acid; hydrogen bromide / 100 °C

7: triethylamine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate / tetrahydrofuran

With hydrogenchloride; tin; potassium peroxymonosulfate; hydrogen bromide; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; acetic acid; triethylamine; tin(ll) chloride; sodium nitrite; In tetrahydrofuran; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2012.10.034

Reference yield:

: 289913-99-1
C₆H₆FN₃O₂

: 1031860-39-5
C₃₂H₂₇F₃N₆O₄

Guidance literature:: Multi-step reaction with 6 steps

1: acetic acid

2: triethylamine / tetrahydrofuran

3: hydrogenchloride; tin / tetrahydrofuran; water

4: potassium peroxymonosulfate / water; N,N-dimethyl-formamide

5: acetic acid; hydrogen bromide / 100 °C

6: triethylamine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate / tetrahydrofuran

With hydrogenchloride; tin; potassium peroxymonosulfate; hydrogen bromide; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; acetic acid; triethylamine; In tetrahydrofuran; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2012.10.034

Reference yield:

: 1415359-43-1
C₁₆H₁₁F₄N₃O₃

: 1031860-39-5
C₃₂H₂₇F₃N₆O₄

Guidance literature:: Multi-step reaction with 5 steps

1: triethylamine / tetrahydrofuran

2: hydrogenchloride; tin / tetrahydrofuran; water

3: potassium peroxymonosulfate / water; N,N-dimethyl-formamide

4: acetic acid; hydrogen bromide / 100 °C

5: triethylamine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate / tetrahydrofuran

With hydrogenchloride; tin; potassium peroxymonosulfate; hydrogen bromide; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; acetic acid; triethylamine; In tetrahydrofuran; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2012.10.034