[[κP,η(2)(P=C)-(1-(2-diphenylphosphinoethyl)-diphenylphosphonio)-3-triphenylphosphonio-benzo[c]phospholide](η(5)-cyclopentadienyl)cobalt(I)] tetraphenyl borate

Base Information

Chemical Name:[[κP,η(2)(P=C)-(1-(2-diphenylphosphinoethyl)-diphenylphosphonio)-3-triphenylphosphonio-benzo[c]phospholide](η(5)-cyclopentadienyl)cobalt(I)] tetraphenyl borate
CAS No.:375396-74-0
Molecular Formula:C₂₄H₂₀B*C₅₇H₄₈CoP₄
Molecular Weight:1235.13
Hs Code.:

[[κP,η(2)(P=C)-(1-(2-diphenylphosphinoethyl)-diphenylphosphonio)-3-triphenylphosphonio-benzo[c]phospholide](η(5)-cyclopentadienyl)cobalt(I)] tetraphenyl borate

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Chemical Property of [[κP,η(2)(P=C)-(1-(2-diphenylphosphinoethyl)-diphenylphosphonio)-3-triphenylphosphonio-benzo[c]phospholide](η(5)-cyclopentadienyl)cobalt(I)] tetraphenyl borate

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Technology Process of [[κP,η(2)(P=C)-(1-(2-diphenylphosphinoethyl)-diphenylphosphonio)-3-triphenylphosphonio-benzo[c]phospholide](η(5)-cyclopentadienyl)cobalt(I)] tetraphenyl borate

There total 1 articles about [[κP,η(2)(P=C)-(1-(2-diphenylphosphinoethyl)-diphenylphosphonio)-3-triphenylphosphonio-benzo[c]phospholide](η(5)-cyclopentadienyl)cobalt(I)] tetraphenyl borate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: η5-cyclopentadienylbis(ethene)cobalt

: 351203-64-0
[1-[(2-diphenylphosphinoethyl)-diphenylphosphonio]-3-triphenylphosphonio-benzo[c]phospholide] tetraphenylborate

: 375396-74-0
[[κP,η(2)(P=C)-(1-(2-diphenylphosphinoethyl)-diphenylphosphonio)-3-triphenylphosphonio-benzo[c]phospholide](η(5)-cyclopentadienyl)cobalt(I)] tetraphenyl borate

Guidance literature:: In tetrahydrofuran; byproducts: C2H4; under dry Ar, thf was condensed onto solid mixt. of equimolar amt. of Co-complex and P-compd. in vac., mixt. was allowed to dissolve at -40 °C, stirring at this temp. for for 1 h and at room temp. for 2 h; soln. was concd. in vac., Et2O was added, ppt. was filtered off, washed with Et2O, dried in vac., elem. anal.;
DOI:10.1002/1521-3749(200109)627:9<2269::AID-ZAAC2269>3.0.CO;2-I

Reference yield:

: 109-99-9,24979-97-3,77392-70-2
tetrahydrofuran

: 110-54-3
hexane

: 375396-74-0
[[κP,η(2)(P=C)-(1-(2-diphenylphosphinoethyl)-diphenylphosphonio)-3-triphenylphosphonio-benzo[c]phospholide](η(5)-cyclopentadienyl)cobalt(I)] tetraphenyl borate

: [[κP,η(2)(P=C)-(1-(2-diphenylphosphinoethyl)-diphenylphosphonio)-3-triphenylphosphonio-benzo[c]phospholide](η(5)-cyclopentadienyl)cobalt(I)] tetraphenyl borate*tetrahydrofurane*0.5n-hexane

Guidance literature:: In tetrahydrofuran; diethyl ether; pentane; under dry Ar; crystn. from THF/Et2O/n-hexane;
DOI:10.1002/1521-3749(200109)627:9<2269::AID-ZAAC2269>3.0.CO;2-I