(4Z,9Z,15Z)-17-Ethyl-1,19-dioxo-3,3,7,8,13,18-hexamethyl-1,2,3,19,23,24-hexahydro-21H-bilin-12-N-<(S)-phenylalaninethylester>-propionsaeureamid

Base Information

• Chemical Name: (4Z,9Z,15Z)-17-Ethyl-1,19-dioxo-3,3,7,8,13,18-hexamethyl-1,2,3,19,23,24-hexahydro-21H-bilin-12-N-<(S)-phenylalaninethylester>-propionsaeureamid
• CAS No.: 100923-25-9
• Molecular Formula: C₄₁H₄₉N₅O₅
• Molecular Weight: 691.871

Synonyms:

Chemical Property of (4Z,9Z,15Z)-17-Ethyl-1,19-dioxo-3,3,7,8,13,18-hexamethyl-1,2,3,19,23,24-hexahydro-21H-bilin-12-N-<(S)-phenylalaninethylester>-propionsaeureamid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (4Z,9Z,15Z)-17-Ethyl-1,19-dioxo-3,3,7,8,13,18-hexamethyl-1,2,3,19,23,24-hexahydro-21H-bilin-12-N-<(S)-phenylalaninethylester>-propionsaeureamid

There total 3 articles about (4Z,9Z,15Z)-17-Ethyl-1,19-dioxo-3,3,7,8,13,18-hexamethyl-1,2,3,19,23,24-hexahydro-21H-bilin-12-N-<(S)-phenylalaninethylester>-propionsaeureamid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

H-Phe-OEt (3081-24-1) → (4Z,9Z,15Z)-17-Ethyl-1,19-dioxo-3,3,7,8,13,18-hexamethyl-1,2,3,19,23,24-hexahydro-21H-bilin-12-N-<(S)-phenylalaninethylester>-propionsaeureamid (100923-25-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 85 percent / 1.) N,N-carbonyldiimidazole / dimethylformamide / 1.) 4 h, room temperature; 2.) 12 h, room temperature

With 1,1'-carbonyldiimidazole; In N,N-dimethyl-formamide;

DOI:10.1007/BF00809198

Reference yield:

(Z)-9-tert-Butoxycarbonyl-3-ethyl-2,7-dimethyl-dipyrrin-1-one-8-propanoic acid (100923-14-6) → (4Z,9Z,15Z)-17-Ethyl-1,19-dioxo-3,3,7,8,13,18-hexamethyl-1,2,3,19,23,24-hexahydro-21H-bilin-12-N-<(S)-phenylalaninethylester>-propionsaeureamid (100923-25-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 85 percent / 1.) N,N-carbonyldiimidazole / dimethylformamide / 1.) 4 h, room temperature; 2.) 12 h, room temperature

With 1,1'-carbonyldiimidazole; In N,N-dimethyl-formamide;

DOI:10.1007/BF00809198

Reference yield:

5-(3,3-dimethyl-5-oxo-pyrrolidin-2-ylidenemethyl)-3,4-dimethyl-1H-pyrrole-2-carboxylic acid tert-butyl ester (84750-73-2) + (Z)-3-Ethyl-3',4-dimethyl-5'-tert-butoxycarbonyl-4'--5-(1H)-2,2'-pyrromethenon (100923-18-0) → (4Z,9Z,15Z)-17-Ethyl-1,19-dioxo-3,3,7,8,13,18-hexamethyl-1,2,3,19,23,24-hexahydro-21H-bilin-12-N-<(S)-phenylalaninethylester>-propionsaeureamid (100923-25-9)

Guidance literature:

Yield given. Multistep reaction;

DOI:10.1007/BF00809198

upstream raw materials:

5-(3,3-dimethyl-5-oxo-pyrrolidin-2-ylidenemethyl)-3,4-dimethyl-1H-pyrrole-2-carboxylic acid tert-butyl ester

(Z)-3-Ethyl-3',4-dimethyl-5'-tert-butoxycarbonyl-4'--5-(1H)-2,2'-pyrromethenon

H-Phe-OEt

(Z)-9-tert-Butoxycarbonyl-3-ethyl-2,7-dimethyl-dipyrrin-1-one-8-propanoic acid

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