Co(CO)3(P(C₆H₅)3)2⁽¹⁺⁾

Base Information

Chemical Name:Co(CO)3(P(C₆H₅)3)2⁽¹⁺⁾
CAS No.:47854-84-2
Molecular Formula:C₃₉H₃₀CoO₃P₂
Molecular Weight:667.606
Hs Code.:

Co(CO)3(P(C<sub>6</sub>H<sub>5</sub>)3)2<sup>(1+)</sup>

Synonyms:

Suppliers and Price of Co(CO)3(P(C₆H₅)3)2⁽¹⁺⁾

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Co(CO)3(P(C₆H₅)3)2⁽¹⁺⁾

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Co(CO)3(P(C₆H₅)3)2⁽¹⁺⁾

There total 6 articles about Co(CO)3(P(C₆H₅)3)2⁽¹⁺⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 17.4%

: Fe2(μ-S)2(CO)6

: 56-34-8
tetraethylammonium chloride

: 3017-60-5
cobalt(II) thiocyanate

: 22560-16-3
lithium triethylborohydride

: 603-35-0
triphenylphosphine

: 325698-60-0,47854-84-2,47854-90-0
Co(CO)3(P(C₆H₅)3)2⁽¹⁺⁾

: 467448-36-8
Co(CO)3(P(C₆H₅)3)2B(C₂H₅)3

: 467222-67-9
(C₂H₅)4N⁽¹⁺⁾*CoFe₂(CO)8S(P(C₆H₅)3)^(1-)=((C₂H₅)4N)(CoFe₂(CO)8S(P(C₆H₅)3))

Guidance literature:: In tetrahydrofuran; acetonitrile; under N2, Schlenk techniques; PPh3 and Et4NCl in MeCN stirred (room temp.); Co(SCN)2 added (soln. A); Fe complex in MeCN stirred (-78°C);LiBHEt3 in THF added dropwise; soln. A added; stirred (> 20 min); warme d to room temp.; stirred for 48 h; filtered; filtrate cooled (4°C, several d); filtered; ppt. washed(i-PrOH); dried in vac.(Co-Fe complex); filtrate concd. by vac.; i-PrOH added; filtered; crystals dried in vac.(Co-B complex); filtrate cooled (4°C, Co complex); elem. anal.;
DOI:10.1016/S0022-328X(02)01568-1

Reference yield:

: 15226-74-1,61091-28-9,61117-58-6
dicobalt octacarbonyl

: 47854-84-2,47854-90-0,325698-60-0
C₃₉H₃₀CoO₃P₂⁽¹⁺⁾

Guidance literature:: With triphenylphosphine; In dichloromethane; 2 equiv. of phosphine, 30 min., room temp. in the dark;

Reference yield:

: 53433-12-8
[bis(triphenylphospine)nitrogen⁽¹⁺⁾][Co(CO)4]

: 47854-84-2,47854-90-0,325698-60-0
C₃₉H₃₀CoO₃P₂⁽¹⁺⁾

: 10170-27-1,190336-13-1
Co₂(CO)6(PPh₃)2

Guidance literature:: With triphenylphosphine; In tetrahydrofuran; byproducts: CO; Electrochem. Process; electrooxidation (-0.30 V vs. SCE, Pt electrode contg. 0.3 M tetrabutylammonium perchlorate); various PPh3 concns. yielded various product ratios; in the dark;