(2-chloro-phenyl)-(8-methyl-[1]naphthyl)-ketone

Base Information

• Chemical Name: (2-chloro-phenyl)-(8-methyl-[1]naphthyl)-ketone
• CAS No.: 855609-78-8
• Molecular Formula: C₁₈H₁₃ClO
• Molecular Weight: 280.754
• Mol file: 855609-78-8.mol

Synonyms:

Chemical Property of (2-chloro-phenyl)-(8-methyl-[1]naphthyl)-ketone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (2-chloro-phenyl)-(8-methyl-[1]naphthyl)-ketone

There total 4 articles about (2-chloro-phenyl)-(8-methyl-[1]naphthyl)-ketone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(2-chloro-phenyl)-(8-methyl-[1]naphthyl)-methanol → (2-chloro-phenyl)-(8-methyl-[1]naphthyl)-ketone (855609-78-8)

Guidance literature:

With sodium dichromate; acetic acid; benzene; weiteres Reagens: Schwefelsaeure;

DOI:10.1021/ja01870a044

Reference yield:

2-Chlorobenzonitrile (873-32-5) → (2-chloro-phenyl)-(8-methyl-[1]naphthyl)-ketone (855609-78-8)

Guidance literature:

With diethyl ether; benzene; Behandeln des Reaktionsgemisches mit verd. wss. Salzsaeure und Erhitzen des Reaktionsprodukts mit wss. Ameisensaeure und geringen Mengen Schwefelsaeure auf 150grad;

DOI:10.1021/ja01870a044

Reference yield:

2-chloro-benzaldehyde (89-98-5) → (2-chloro-phenyl)-(8-methyl-[1]naphthyl)-ketone (855609-78-8)

Guidance literature:

Multi-step reaction with 2 steps

1: diethyl ether; benzene

2: benzene; Na₂Cr₂O₇; aqueous acetic acid / weiteres Reagens: Schwefelsaeure

With sodium dichromate; diethyl ether; acetic acid; benzene;

DOI:10.1021/ja01870a044

upstream raw materials:

2-chlorophenylmagnesium bromide

2-Chlorobenzonitrile

2-chloro-benzaldehyde

Downstream raw materials:

1-[1-(2-chloro-phenyl)-vinyl]-8-methyl-naphthalene