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4,4'-Azobistriphenylmethan

Base Information
  • Chemical Name:4,4'-Azobistriphenylmethan
  • CAS No.:128527-48-0
  • Molecular Formula:C38H30N2
  • Molecular Weight:514.67
  • Hs Code.:
4,4'-Azobistriphenylmethan

Synonyms:

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Chemical Property of 4,4'-Azobistriphenylmethan
Chemical Property:
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Technology Process of 4,4'-Azobistriphenylmethan

There total 2 articles about 4,4'-Azobistriphenylmethan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
Multi-step reaction with 2 steps
1: NaOH, Zn-dust / 2-methoxy-ethanol; methanol; H2O / 1 h / Heating
2: CrO3, glacial AcOH / 1) 1 h, 100 deg C 2) 24 h, r.t.
With chromium(VI) oxide; sodium hydroxide; acetic acid; zinc; In methanol; 2-methoxy-ethanol; water;
Guidance literature:
Multi-step reaction with 3 steps
1: 69 percent / conc. H2SO4 / 48 h
2: NaOH, Zn-dust / 2-methoxy-ethanol; methanol; H2O / 1 h / Heating
3: CrO3, glacial AcOH / 1) 1 h, 100 deg C 2) 24 h, r.t.
With chromium(VI) oxide; sodium hydroxide; sulfuric acid; acetic acid; zinc; In methanol; 2-methoxy-ethanol; water;
Guidance literature:
Multi-step reaction with 2 steps
1: 73 percent / conc. HNO3, NaNO2 / dioxane; H2O / 100 °C
2: 73 percent / m-chloroperbenzoic acid / CH2Cl2 / 3 h / Heating
With nitric acid; 3-chloro-benzenecarboperoxoic acid; sodium nitrite; In 1,4-dioxane; dichloromethane; water;
upstream raw materials:

1-(diphenylmethyl)-4-nitrobenzene

4-nitrobenzaldehdye

Downstream raw materials:

4,4'-Azoxybistritanol

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