4'-Nitrobenzoin benzoate

Base Information

• Chemical Name: 4'-Nitrobenzoin benzoate
• CAS No.: 119123-53-4
• Molecular Formula: C₂₁H₁₅NO₅
• Molecular Weight: 361.354
• Mol file: 119123-53-4.mol

Synonyms:

Chemical Property of 4'-Nitrobenzoin benzoate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4'-Nitrobenzoin benzoate

There total 5 articles about 4'-Nitrobenzoin benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

benzoyl chloride (98-88-4) + 2-Hydroxy-2-(4-nitro-phenyl)-1-phenyl-ethanone (119123-52-3) → 4'-Nitrobenzoin benzoate (119123-53-4) + 4-Nitrostilbenediol-4'-nitrodibenzoate

Guidance literature:

With pyridine; at 80 ℃; for 1h;

DOI:10.1055/s-1988-27712

Reference yield:

4'-Nitrobenzoin acetate (119123-51-2) → 4'-Nitrobenzoin benzoate (119123-53-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 10percent aq. H₂SO₄ / 15 h / Ambient temperature

2: 39 percent / pyridine / 1 h / 80 °C

With pyridine; sulfuric acid;

DOI:10.1055/s-1988-27712

Reference yield:

1,2-diphenyl-2-oxoethyl benzoate (1459-20-7) → 4'-Nitrobenzoin benzoate (119123-53-4)

Guidance literature:

With nitric acid;

upstream raw materials:

1,2-diphenyl-2-oxoethyl benzoate

benzoyl chloride

2-Hydroxy-2-(4-nitro-phenyl)-1-phenyl-ethanone

4'-Nitrobenzoin acetate

Refernces