5-<4-(4-Dimethylaminophenyl)-2-azabuta-1,3-dienyl>-4-<6-(4-dimethylaminophenyl)-1,2-dimethyl-4-oxo-1-azahexa-2,5-dienylidenium>-1-methyl-4H-imidazolium diiodide

Base Information

• Chemical Name: 5-<4-(4-Dimethylaminophenyl)-2-azabuta-1,3-dienyl>-4-<6-(4-dimethylaminophenyl)-1,2-dimethyl-4-oxo-1-azahexa-2,5-dienylidenium>-1-methyl-4H-imidazolium diiodide
• CAS No.: 73566-85-5
• Molecular Formula: C₃₀H₃₆N₆O*2I
• Molecular Weight: 750.464
• Mol file: 73566-85-5.mol

Synonyms:

Chemical Property of 5-<4-(4-Dimethylaminophenyl)-2-azabuta-1,3-dienyl>-4-<6-(4-dimethylaminophenyl)-1,2-dimethyl-4-oxo-1-azahexa-2,5-dienylidenium>-1-methyl-4H-imidazolium diiodide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 5-<4-(4-Dimethylaminophenyl)-2-azabuta-1,3-dienyl>-4-<6-(4-dimethylaminophenyl)-1,2-dimethyl-4-oxo-1-azahexa-2,5-dienylidenium>-1-methyl-4H-imidazolium diiodide

There total 3 articles about 5-<4-(4-Dimethylaminophenyl)-2-azabuta-1,3-dienyl>-4-<6-(4-dimethylaminophenyl)-1,2-dimethyl-4-oxo-1-azahexa-2,5-dienylidenium>-1-methyl-4H-imidazolium diiodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

caffeidine (20041-90-1) → 5-<4-(4-Dimethylaminophenyl)-2-azabuta-1,3-dienyl>-4-<6-(4-dimethylaminophenyl)-1,2-dimethyl-4-oxo-1-azahexa-2,5-dienylidenium>-1-methyl-4H-imidazolium diiodide (73566-85-5)

Guidance literature:

Multi-step reaction with 2 steps

1: methanol

2: 67percent aq. HI / methanol / 6 h / Heating

With hydrogen iodide; In methanol;

DOI:10.1002/ardp.19803130211

Reference yield:

acetylacetone (123-54-6,81235-32-7) → 5-<4-(4-Dimethylaminophenyl)-2-azabuta-1,3-dienyl>-4-<6-(4-dimethylaminophenyl)-1,2-dimethyl-4-oxo-1-azahexa-2,5-dienylidenium>-1-methyl-4H-imidazolium diiodide (73566-85-5)

Guidance literature:

Multi-step reaction with 2 steps

1: methanol

2: 67percent aq. HI / methanol / 6 h / Heating

With hydrogen iodide; In methanol;

DOI:10.1002/ardp.19803130211

Reference yield:

3-Methyl-5-[methyl-((E)-1-methyl-3-oxo-but-1-enyl)-amino]-3H-imidazole-4-carboxylic acid methylamide + 4-dimethylamino-benzaldehyde (100-10-7) → 5-<4-(4-Dimethylaminophenyl)-2-azabuta-1,3-dienyl>-4-<6-(4-dimethylaminophenyl)-1,2-dimethyl-4-oxo-1-azahexa-2,5-dienylidenium>-1-methyl-4H-imidazolium diiodide (73566-85-5)

Guidance literature:

With hydrogen iodide; In methanol; for 6h; Yield given; Heating;

DOI:10.1002/ardp.19803130211

upstream raw materials:

4-dimethylamino-benzaldehyde

caffeidine

acetylacetone