4-[4-(4-Hydroxy-phenoxy)-butoxy]-benzoic acid

Base Information

Chemical Name:4-[4-(4-Hydroxy-phenoxy)-butoxy]-benzoic acid
CAS No.:150566-21-5
Molecular Formula:C₁₇H₁₈O₅
Molecular Weight:302.327
Hs Code.:

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Chemical Property of 4-[4-(4-Hydroxy-phenoxy)-butoxy]-benzoic acid

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Technology Process of 4-[4-(4-Hydroxy-phenoxy)-butoxy]-benzoic acid

There total 7 articles about 4-[4-(4-Hydroxy-phenoxy)-butoxy]-benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4-[4-(4-Benzyloxy-phenoxy)-butoxy]-benzoic acid

: 150566-21-5
4-[4-(4-Hydroxy-phenoxy)-butoxy]-benzoic acid

Guidance literature:: With hydrogen; 5%-palladium/activated carbon; In various solvent(s); Ambient temperature;

Reference yield:

: 120-47-8
Ethyl 4-hydroxybenzoate

: 150566-21-5
4-[4-(4-Hydroxy-phenoxy)-butoxy]-benzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / cyclohexanone / 6 h / Heating

2: potassium hydroxide / ethanol; H₂O / 6 h / Heating

3: hydrogen / Pd-5percent on charcoal / various solvent(s) / Ambient temperature

With potassium hydroxide; hydrogen; potassium carbonate; 5%-palladium/activated carbon; In ethanol; water; cyclohexanone;

Reference yield:

: 103-16-2
4-Benzyloxyphenol

: 150566-21-5
4-[4-(4-Hydroxy-phenoxy)-butoxy]-benzoic acid

Guidance literature:: Multi-step reaction with 6 steps

1: potassium carbonate / cyclohexanone / 4 h / Heating

2: lithium aluminium hydride / diethyl ether / 4 h / Heating

3: pyridine / 12 h / 0 °C

4: potassium carbonate / cyclohexanone / 6 h / Heating

5: potassium hydroxide / ethanol; H₂O / 6 h / Heating

6: hydrogen / Pd-5percent on charcoal / various solvent(s) / Ambient temperature

With pyridine; potassium hydroxide; lithium aluminium tetrahydride; hydrogen; potassium carbonate; 5%-palladium/activated carbon; In diethyl ether; ethanol; water; cyclohexanone;