triphenyltin hydrosulfide

Base Information

• Chemical Name: triphenyltin hydrosulfide
• CAS No.: 33364-67-9
• Molecular Formula: C₁₈H₁₆SSn
• Molecular Weight: 383.101
• Mol file: 33364-67-9.mol

Synonyms:

Chemical Property of triphenyltin hydrosulfide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of triphenyltin hydrosulfide

There total 1 articles about triphenyltin hydrosulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.0%

thiophosgene (463-71-8) + triphenyltin(IV) hydroxide (76-87-9) → triphenyltin hydrosulfide (33364-67-9)

Guidance literature:

With Et₃N; H₂O; In benzene; byproducts: CO2, HCl; stirred suspn. of Ph3SnOH and Et3N (1:1) in benzene treated with 1 equiv. of CSCl2 in benzene, stirred at 6°C for 4 h, treated with H2O, stirred at room temp. for 1 d (mechanism discussed); filtered, dried (vac.), dissolved (Et2O), filtered, left overnight, elem. anal.;

DOI:10.1016/j.ica.2010.12.014

upstream raw materials:

thiophosgene

triphenyltin(IV) hydroxide