C₈H₁₁IO₅

Base Information

Chemical Name:C₈H₁₁IO₅
CAS No.:1311379-47-1
Molecular Formula:C₈H₁₁IO₅
Molecular Weight:314.077
Hs Code.:

C<sub>8</sub>H<sub>11</sub>IO<sub>5</sub>

Synonyms:

Suppliers and Price of C₈H₁₁IO₅

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₈H₁₁IO₅

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₈H₁₁IO₅

There total 10 articles about C₈H₁₁IO₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1311379-29-9
C₂₂H₂₃IO₅

: 1311379-47-1
C₈H₁₁IO₅

Guidance literature:: With boron trichloride; In dichloromethane; at -78 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ja203642n

Reference yield:

: 1311379-26-6
C₁₅H₁₈O₅

: 1311379-47-1
C₈H₁₁IO₅

Guidance literature:: Multi-step reaction with 5 steps

1: toluene-4-sulfonic acid / tetrahydrofuran / 80 °C / Inert atmosphere

2: chloro-trimethyl-silane; sodium cyanoborohydride / acetonitrile / 0 °C / Inert atmosphere; Heating

3: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / 3 h / 80 °C / Inert atmosphere

4: magnesium iodide / dichloromethane / -78 - -20 °C / Inert atmosphere

5: boron trichloride / dichloromethane / 1 h / -78 °C / Inert atmosphere

With chloro-trimethyl-silane; boron trichloride; sodium cyanoborohydride; toluene-4-sulfonic acid; magnesium iodide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; dichloromethane; ethyl acetate; acetonitrile; 4: intramolecular halo-Michael aldol reaction;
DOI:10.1021/ja203642n

Reference yield:

: C₁₇H₂₀O₄

: 1311379-47-1
C₈H₁₁IO₅

Guidance literature:: Multi-step reaction with 7 steps

1: sodium chlorite; sodium phosphate monobasic monohydrate / 2-methyl-but-2-ene; water; tert-butyl alcohol / 0 °C

2: sulfuric acid / 0 - 20 °C / Inert atmosphere

3: toluene-4-sulfonic acid / tetrahydrofuran / 80 °C / Inert atmosphere

4: chloro-trimethyl-silane; sodium cyanoborohydride / acetonitrile / 0 °C / Inert atmosphere; Heating

5: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / 3 h / 80 °C / Inert atmosphere

6: magnesium iodide / dichloromethane / -78 - -20 °C / Inert atmosphere

7: boron trichloride / dichloromethane / 1 h / -78 °C / Inert atmosphere

With sodium chlorite; chloro-trimethyl-silane; sodium phosphate monobasic monohydrate; sulfuric acid; boron trichloride; sodium cyanoborohydride; toluene-4-sulfonic acid; magnesium iodide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; 2-methyl-but-2-ene; dichloromethane; water; ethyl acetate; acetonitrile; tert-butyl alcohol; 1: Pinnick oxidation / 6: intramolecular halo-Michael aldol reaction;
DOI:10.1021/ja203642n