C₄₄H₃₂N₈Pd

Base Information

• Chemical Name: C₄₄H₃₂N₈Pd
• CAS No.: 1214741-98-6
• Molecular Formula: C₄₄H₃₂N₈Pd
• Molecular Weight: 779.212
• Mol file: 1214741-98-6.mol

Synonyms:

Chemical Property of C₄₄H₃₂N₈Pd

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₄H₃₂N₈Pd

There total 2 articles about C₄₄H₃₂N₈Pd which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

tetrakis-5,10,15,20-(o-aminophenyl)porphyrin (52199-35-6) → C44H32N8Pd (1214741-98-6)

Guidance literature:

tetrakis-5,10,15,20-(o-aminophenyl)porphyrin; With tetra(n-butyl)ammonium hydroxide; palladium diacetate; In methanol; dichloromethane; for 9h; Reflux; Inert atmosphere; Darkness;

With silica gel; In toluene; for 20h; Inert atmosphere; Darkness; Reflux;

DOI:10.1039/b920676k

Reference yield: 24.0%

palladium diacetate (3375-31-3) + cis-α,α,α,α-atropisomer 5,10,15,20-tetrakis(2-aminophenyl)porphyrin (52199-35-6,68070-27-9,68070-28-0,68070-29-1,68070-30-4) → meso-tetrakis(o-aminophenyl)porphyrin Pd complex (1214741-98-6)

Guidance literature:

In CHCl₃; methanol; mixt. of atropoisomers (enriched in α4 upon heating in toluene in presence silica) refluxed in CHCl3 and MeOH; chromy. on alumina;

DOI:10.1039/b920676k

upstream raw materials:

palladium diacetate

cis-α,α,α,α-atropisomer 5,10,15,20-tetrakis(2-aminophenyl)porphyrin

tetrakis-5,10,15,20-(o-aminophenyl)porphyrin