N-(4-iodophenyl)-N'-phenylbenzenecarbohydrazonamide

Base Information

• Chemical Name: N-(4-iodophenyl)-N'-phenylbenzenecarbohydrazonamide
• CAS No.: 1244508-15-3
• Molecular Formula: C₁₉H₁₆IN₃
• Molecular Weight: 413.261
• Mol file: 1244508-15-3.mol

Synonyms:

Chemical Property of N-(4-iodophenyl)-N'-phenylbenzenecarbohydrazonamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-(4-iodophenyl)-N'-phenylbenzenecarbohydrazonamide

There total 1 articles about N-(4-iodophenyl)-N'-phenylbenzenecarbohydrazonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

N-phenylbenzohydrazonoyl chloride (15424-14-3) + p-aminoiodobenzene (540-37-4) → N-(4-iodophenyl)-N'-phenylbenzenecarbohydrazonamide (1244508-15-3,1421278-01-4)

Guidance literature:

In benzene; for 8h; Reflux;

DOI:10.1055/s-0029-1218782

Reference yield: 81.0%

N-(4-iodophenyl)-N'-phenylbenzenecarbohydrazonamide (1244508-15-3,1421278-01-4) → 7-iodo-1,3-diphenyl-1,4-dihydrobenzo[e][1,2,4]triazin-4-yl (1244508-25-5)

Guidance literature:

With 10% palladium on activated charcoal; 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 20 ℃;

DOI:10.1039/c1ob05167a

Reference yield: 81.0%

N-(4-iodophenyl)-N'-phenylbenzenecarbohydrazonamide (1244508-15-3,1421278-01-4) → 7-iodo-1,3-diphenyl-1,4-dihydrobenzo[e][1,2,4]triazin-4-yl (1244508-25-5,1421277-98-6)

Guidance literature:

With 5% Pd(II)/C(eggshell); 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 20 ℃; for 6h;

DOI:10.1055/s-0029-1218782

upstream raw materials:

N-phenylbenzohydrazonoyl chloride

p-aminoiodobenzene

Downstream raw materials:

7-iodo-1,3-diphenyl-1,4-dihydrobenzo[e][1,2,4]triazin-4-yl

7-iodo-1,3-diphenyl-1,4-dihydrobenzo[e][1,2,4]triazin-4-yl

1,3-diphenyl-7-(4-phenyl)-1,4-dihydro-1,2,4-benzotriazin-4-yl

1,3-diphenylbenzo[e]-[1,2,4]triazin-7(1H)-one