1-<2-(N-benzyl-N-methylamino)ethyl>-1-methyl-2-tetralone ethylene acetal

Base Information

Chemical Name:1-<2-(N-benzyl-N-methylamino)ethyl>-1-methyl-2-tetralone ethylene acetal
CAS No.:88207-66-3
Molecular Formula:C₂₃H₂₉NO₂
Molecular Weight:351.489
Hs Code.:

Synonyms:

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Chemical Property of 1-<2-(N-benzyl-N-methylamino)ethyl>-1-methyl-2-tetralone ethylene acetal

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Technology Process of 1-<2-(N-benzyl-N-methylamino)ethyl>-1-methyl-2-tetralone ethylene acetal

There total 5 articles about 1-<2-(N-benzyl-N-methylamino)ethyl>-1-methyl-2-tetralone ethylene acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 107-21-1
ethylene glycol

: 88207-60-7
1-<2-(N-benzyl-N-methylamino)ethyl>-1-methyl-2-tetralone

: 88207-66-3
1-<2-(N-benzyl-N-methylamino)ethyl>-1-methyl-2-tetralone ethylene acetal

Guidance literature:: With toluene-4-sulfonic acid; In toluene; for 6h; Heating;
DOI:10.1039/P19830002583

Reference yield:

: 4024-14-0
1-methyl-2-tetralone

: 88207-66-3
1-<2-(N-benzyl-N-methylamino)ethyl>-1-methyl-2-tetralone ethylene acetal

Guidance literature:: Multi-step reaction with 3 steps

1: 68 percent / sodamide

2: 72 percent / dimethylformamide / 24 h / Heating

3: 75 percent / p-TsOH / toluene / 6 h / Heating

With toluene-4-sulfonic acid; sodium amide; In N,N-dimethyl-formamide; toluene;
DOI:10.1039/P19830002583

Reference yield:

: 88207-56-1
1-<2-(N,N-dimethylamino)ethyl>-1-methyl-2-tetralone

: 88207-66-3
1-<2-(N-benzyl-N-methylamino)ethyl>-1-methyl-2-tetralone ethylene acetal

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / dimethylformamide / 24 h / Heating

2: 75 percent / p-TsOH / toluene / 6 h / Heating

With toluene-4-sulfonic acid; In N,N-dimethyl-formamide; toluene;
DOI:10.1039/P19830002583