5-(2,3-dihydrobenzo[b][1,4]dioxin-6-yl)-5-ethyl-3-(4-(4-(1,1,1,3,3,3-hexafluoro-2-hydroxypropan-2-yl)-2-n-propylphenoxy)butyl)imidazolidine-2,4-dione

Base Information

Chemical Name:5-(2,3-dihydrobenzo[b][1,4]dioxin-6-yl)-5-ethyl-3-(4-(4-(1,1,1,3,3,3-hexafluoro-2-hydroxypropan-2-yl)-2-n-propylphenoxy)butyl)imidazolidine-2,4-dione
CAS No.:1031396-51-6
Molecular Formula:C₂₉H₃₂F₆N₂O₆
Molecular Weight:618.573
Hs Code.:

5-(2,3-dihydrobenzo[b][1,4]dioxin-6-yl)-5-ethyl-3-(4-(4-(1,1,1,3,3,3-hexafluoro-2-hydroxypropan-2-yl)-2-n-propylphenoxy)butyl)imidazolidine-2,4-dione

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Chemical Property of 5-(2,3-dihydrobenzo[b][1,4]dioxin-6-yl)-5-ethyl-3-(4-(4-(1,1,1,3,3,3-hexafluoro-2-hydroxypropan-2-yl)-2-n-propylphenoxy)butyl)imidazolidine-2,4-dione

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Technology Process of 5-(2,3-dihydrobenzo[b][1,4]dioxin-6-yl)-5-ethyl-3-(4-(4-(1,1,1,3,3,3-hexafluoro-2-hydroxypropan-2-yl)-2-n-propylphenoxy)butyl)imidazolidine-2,4-dione

There total 14 articles about 5-(2,3-dihydrobenzo[b][1,4]dioxin-6-yl)-5-ethyl-3-(4-(4-(1,1,1,3,3,3-hexafluoro-2-hydroxypropan-2-yl)-2-n-propylphenoxy)butyl)imidazolidine-2,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₁H₃₆F₆N₂O₇

: 1031396-51-6
5-(2,3-dihydrobenzo[b][1,4]dioxin-6-yl)-5-ethyl-3-(4-(4-(1,1,1,3,3,3-hexafluoro-2-hydroxypropan-2-yl)-2-n-propylphenoxy)butyl)imidazolidine-2,4-dione

Guidance literature:: With hydrogenchloride; In ethyl acetate; at 20 ℃;
DOI:10.1016/j.bmcl.2015.04.080

Reference yield:

: 20632-12-6
1-(2,3-dihydrobenzo[b][1,4]dioxin-6-yl)propan-1-one

: 1031396-51-6
5-(2,3-dihydrobenzo[b][1,4]dioxin-6-yl)-5-ethyl-3-(4-(4-(1,1,1,3,3,3-hexafluoro-2-hydroxypropan-2-yl)-2-n-propylphenoxy)butyl)imidazolidine-2,4-dione

Guidance literature:: Multi-step reaction with 3 steps

1.1: water; ethanol / 70 °C

2.1: potassium carbonate / N,N-dimethyl-formamide / 20 °C

2.2: 20 °C

3.1: hydrogenchloride / ethyl acetate / 20 °C

With hydrogenchloride; potassium carbonate; In ethanol; water; ethyl acetate; N,N-dimethyl-formamide; 1.1: |Bucherer-Bergs Reaction;
DOI:10.1016/j.bmcl.2015.04.080

Reference yield:

: 493-09-4
benzo-1,4-dioxane

: 1031396-51-6
5-(2,3-dihydrobenzo[b][1,4]dioxin-6-yl)-5-ethyl-3-(4-(4-(1,1,1,3,3,3-hexafluoro-2-hydroxypropan-2-yl)-2-n-propylphenoxy)butyl)imidazolidine-2,4-dione

Guidance literature:: Multi-step reaction with 4 steps

1.1: aluminum (III) chloride; carbonic acid dimethyl ester / 20 °C

2.1: water; ethanol / 70 °C

3.1: potassium carbonate / N,N-dimethyl-formamide / 20 °C

3.2: 20 °C

4.1: hydrogenchloride / ethyl acetate / 20 °C

With hydrogenchloride; aluminum (III) chloride; potassium carbonate; carbonic acid dimethyl ester; In ethanol; water; ethyl acetate; N,N-dimethyl-formamide; 1.1: |Friedel-Crafts Acylation / 2.1: |Bucherer-Bergs Reaction;
DOI:10.1016/j.bmcl.2015.04.080