2-Methyl-1,3-diphenyl-propane-2-sulfonic acid (3aR,5R,6S,6aR)-5-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl ester

Base Information

Chemical Name:2-Methyl-1,3-diphenyl-propane-2-sulfonic acid (3aR,5R,6S,6aR)-5-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl ester
CAS No.:79697-99-7
Molecular Formula:C₂₈H₃₆O₈S
Molecular Weight:532.655
Hs Code.:

2-Methyl-1,3-diphenyl-propane-2-sulfonic acid (3aR,5R,6S,6aR)-5-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl ester

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Chemical Property of 2-Methyl-1,3-diphenyl-propane-2-sulfonic acid (3aR,5R,6S,6aR)-5-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl ester

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Technology Process of 2-Methyl-1,3-diphenyl-propane-2-sulfonic acid (3aR,5R,6S,6aR)-5-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl ester

There total 2 articles about 2-Methyl-1,3-diphenyl-propane-2-sulfonic acid (3aR,5R,6S,6aR)-5-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 79697-98-6
3-O-(ethylsulfonyl)-1,2-:5,6-di-O-isopropylidene-α-D-glucofuranose

: 100-44-7
benzyl chloride

: 79697-99-7
2-Methyl-1,3-diphenyl-propane-2-sulfonic acid (3aR,5R,6S,6aR)-5-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl ester

Guidance literature:: With potassium hydroxide; In N,N-dimethyl-formamide; at 30 - 35 ℃; for 1h;
DOI:10.1016/S0008-6215(00)81881-9

Reference yield:

: 5450-26-0
1,2,5,6-di-O-isopropylidene-3-O-methylsulfonyl-α-D-glucofuranose

: 79697-99-7
2-Methyl-1,3-diphenyl-propane-2-sulfonic acid (3aR,5R,6S,6aR)-5-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 44 percent / potassium hydroxide / dimethylformamide / 1 h / 35 - 38 °C

2: potassium hydroxide / dimethylformamide / 1 h / 30 - 35 °C

With potassium hydroxide; In N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(00)81881-9